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i <br /> I I 110 2nd Avenue South,#D7 Pacheco CA 94553 5560 <br /> McCampbell Analytical Talc Telephone 925-798-1620 Fax 925-798-1622 <br /> http!lwww mccbell cont E-mal mam c bell com <br /> • AES Regulatory Services, Inc Client Project lD Canteen Corporation Date Sampled 02/13/03 <br /> 2013 Wells Branch Pkwy, <br /> Ste 206 Date Received 02/14/03 <br /> Client Contact Enc Muehlberger Date Extracted 02/15/03-02/18103 <br /> Austin,TX 78728 <br /> Client P O Date Analyzed 02/15/03-02/18103 <br /> Oxygenates and BTEX by GCIMS* <br /> I Analytical Method SW6260B Work Order 0302195 <br /> Extraction Method SW5030B <br /> Lab ID 0302195-005B 0302195-006B 0302195-007B <br /> 1 <br /> I Client ID MW13 MW13A MW13B I Reporting Limit for <br /> ' DF=1 <br /> Matrix W W W <br /> DF 1000 1 I 1 S W <br /> I <br /> Compound <br /> Concentration ugfkg µPQ <br /> IND<500 I ND ND NA 0 5 <br /> ten-Amy]methyl ether(TAME) <br /> NA 0 5 <br /> Benzene <br /> 16,000 ND ND <br /> t-Butyl alcohol(TBA) <br /> ND<5000 ND ND NA 5 0 <br /> NA 0 5 <br /> 1,2-Dibrvmaethane(EDB) <br /> ND<500 ND ND <br /> 1,2-Dichlomethane(1 2-DCA) <br /> ND<500 ND ND NA 05 <br /> Diisopropy]ether(D1PE) <br /> ND<500 ND ND NA 0 5 <br /> Ethylbenzene <br /> 1200 ND ND NA I 0 5 <br /> Ethyl Cert-butyl ether(ET$E) <br /> ND<500 ND ND NA 0 5 <br /> Methyl-t-butyl ether(MTBE) <br /> 1600 ND ND NA 05 <br /> I 26,000 0 55 ND NA 05 <br /> Toluene <br /> 14,000 ND ND NA 05 <br /> Xylenes <br /> Surrogate Recoveries(%) <br /> %SSI 964 113 113 <br /> %5S2 117 115 116 <br /> %SS3 973 96 6 98 7 <br /> Comments <br /> "water and vapor samples and all TCLP&SPLP extracts are reported inµg/L,s(iiVsludgelsolid samples inµg/kg wipe samples inµg/wipe, <br /> Iproduct/oil/non-aqueous liquid samples to mg/L <br /> ND means not detected above the reporting limit,NIA means analyte not applicable to this analysis <br /> I h)lighter than water immiscible sheeniproduct is present,i)liquid sample that contains greater than—2 vol %sediment,l)sample diluted due to high <br /> organic content <br /> DHS Certification No 1644 Angela Rydehus,Lab Manager <br />