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Lancaster . <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster PA 176052425•717-656-2300 Fax 717 65Cr2681•www lancasterlabs com <br /> Page 4 of 5 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 861663 <br /> Reported 08/15/03 at 02 56 PM <br /> Surrogate Quality Control <br /> 4093670 86 <br /> 4093671 82 <br /> 4093672 81 <br /> 4093673 91 <br /> Blank 82 <br /> LCS 106 <br /> MS 110 <br /> MSD 114 <br /> Limits 57-146 <br /> Analysis Name TPH-GRO - Waters <br /> Batch number 03217A07C <br /> Trifluorotoluene-F <br /> 4093674 91 <br /> Blank 82 <br /> LCS 106 <br /> Ms 110 <br /> MSD 114 <br /> Limits 57-146 <br /> Analysis Name Methanol and Ethanol <br /> Batch number 032200023A <br /> Acetone <br /> 4093670 100 <br /> 4093671 104 <br /> 4093672 100 <br /> 4093673 98 <br /> Blank 101 <br /> LCS 100 <br /> MS 100 <br /> MSB 100 <br /> Limits 72-128 <br /> Analysis Name BTEX+MTBE by 8260E <br /> Batch number P032222AA <br /> Dlbromofluoromethane 1 2-Dlchloroethane-d4 Toluene-de 4-Bromofluorobenzene <br /> 4093665 100 96 95 93 <br /> 4093666 102 102 97 94 <br /> 4093667 101 100 97 94 <br /> 4093668 103 101 95 94 <br /> 4093669 101 100 97 94 <br /> 4093674 101 97 97 93 <br /> Blank 102 97 96 94 <br /> LCS 99 92 97 98 <br /> MS 90 92 97 99 <br /> MSD 87 94 97 97 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB+ETOH <br /> Batch number P032252AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> • (2) The background result was more than four times the spike added <br />