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COLUMBIA ANALYTICAL SERVICES, INC <br /> Analytical Report <br /> Client EMCON Associates Service Request S941494 <br /> Project TOSCO 4 1 1 194/0952-092 02 Date Collected 11/17/94 <br /> Sample Matrix Water Date Received 11/21/94 <br /> Date Extracted 11/28/94 <br /> Date Analyzed 12/1,2/94 <br /> Hydrocarbon Scan <br /> EPA Method 3510/Caltforrua DHS LUFT Method <br /> Units ug/L, (ppb) <br /> Mineral TPH as <br /> Analyte Spints Jet Fuel Kerosene Diesel Hydraulic Oil <br /> Method Reporting Limit 50 50 50 50 250 <br /> Sample Name Lab Code <br /> 11194-HPl-W 5941494-001 ND ND ND ND 540 <br /> 11194-HP2-W 5941494-002 160 * ND ND 2,500 ** 340 <br /> 11194-HP3-W 5941494-003 ND ND ND ND 300 <br /> 11194-OBS-W-W S941494-004 ND ND ND ND ND <br /> 11194-OBS-E-W 5941494-005 ND ND ND ND 370 <br /> Method BIank S941128-WB ND ND ND ND ND <br /> * This sample contains components eluting in the mineral spirits range,quantified as mineral spirits The chromatogram <br /> does not match the typical mineral spirits fingerprint <br /> ** This sample contains components eluting in the diesel range, quantified as diesel The chromatogram does not <br /> match the typical diesel fingerprint <br /> n <br /> Approved By jl/1/i �4 <br /> Date <br /> SAM63694 <br /> Page 3 of 9 <br />