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I110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCANDBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> hM2.//www,mccaml2bell.com E-mail main@mccampbell com <br /> I <br /> Date Sampled 08/13/98 <br /> I Advanced GeoEnvironmental Client Project ID Chase-Van Buren <br /> 4005 North Wilson Way <br /> Date Received 08/14/98 <br /> Stockton,CA 95205 Client Contact Kevin McKibben Date Extracted 08/17-08/18/98 <br /> Client P O Date Analyzed 08/17-08/18198 <br /> I Volatile Organics By GC/MS <br /> EPA method 8260 <br /> Lab 1D 93467 <br /> Client ID MW-918-13-98 <br /> Matrix W <br /> Compound Concentration* Compound Concentration* <br /> Acetone NI3<20 Ethylbenzene 2200 <br /> I Benzene 670 Hexachlorobutadiene ND<10 <br /> Bromobenzene ND<10 lodomethane ND<10 <br /> Bromochloromethane ND<10 Isopropylbenzene 83 <br /> I Bromodichloromethane ND<10 p-Isopropyl toluene ND<10 <br /> Bromoform ND<10 Methyl butyl ketone NIX10 <br /> Bromomethane ND<10 Methylene Chloride"' ND<20 <br /> n-Butyl benzene 29 Methyl ethyl ketone ND<10 <br /> sec-Butyl benzene 18 Methyl isobutyl ketone ND<10 <br /> I tert-Butyl benzene ND<10 Methyl tert-Butyl Ether(MTBE) -- <br /> Carbon Disulfide ND<10 Napthalene ND<200 <br /> Carbon Tetrachloride ND<10 n-Propyl benzene 230 <br /> I• Chlorobenzene ND<10 Styrene ND<10 <br /> Chloroethane ND<10 1,1,1,2-Tetrachloroethane ND<10 <br /> 2-Chloroethyl Vinyl Ether") ND<10 1,1,2,2-Tetrachloroethane ND<10 <br /> Chloroform ND<10 Tetrachloroethene ND<10 <br /> I Chloromethane ND<10 Toluene 2900 <br /> 2-Chlorotoluene ND<10 1,2,3-Tnchlorobenzene ND<10 <br /> 4-Chlorotoluene ND<10 1,2,4-Tnchlorobenzene ND<10 <br /> Dibrornochloromeihane ND<10 1,1,1-Tnchloroethane ND<10 <br /> I 1,2-Dbromo-3-chloropropane ND<10 1,1,2-Tnchloroethane NIX10 <br /> Dibromomethane ND<10 Trichloroethene ND<10 <br /> 1,2-Dichlorobenzene NIX10 Trichlorofluoromethane NIX10 <br /> 1,3-Dichlorobenzene ND<10 1,1,3-Tnchloropropane ND<10 <br /> 1,4-Dichlorobenzene ND<10 1,2,4-Tnmethylbenzene 2200 <br /> Dichlorodifluoromethane ND<10 1,3,5-Tnnwthylbmzcne 410 <br /> 1,1-Dichloroethane NIX10 Vinyl Acetate m 110 <br /> 1,2-Dichloroethane ND<10 Vinyl Chloride ° ND<10 <br /> IJ-Dichloroethene ND<10 Xylenes,total 7300 <br /> cis-1,2-Dichlotoethene ND<10 <br /> trans-1,2-Dichl oroethene ND<10 <br /> 1,2-Dichlorepropane ND<10 <br /> I 1,3-Dichloropropane ND<10 <br /> 2,2-Dichlorapropane ND<10 Comments <br /> 1,1-Dichloropropene ND<10 Surrogate Recoveries(%) <br /> cis-1,3-Dichloropropene ND<10 Dibromofluoromethane 99 <br /> I trans-1,3-Dichloropropene ND<10 Toluene-d8 98 <br /> Ethylene dibromide I ND<10 4-Broiriofluorobenzene 97 <br /> "water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 10 ug/L., vapor samples 0 5 ug/L, solid and sludge samples 5 ug/kg, wipes <br /> 0 2ug/wipe ND means not detected above the reporting limit,N/A means analyte not applicable to this analysis <br /> (b) 2 propanone or dimethyl ketone, (c) (2-chloroethoxy)ethene, (d) 2-hexanone, (e) dichloromethane, (f) 2-butanone, (g) 4-methyl-2- <br /> pentanone or isopropylacewne, (h)lighter than water immiscible sheen is present, (i)liquid sample that contains greater than —5 vol % <br /> sediment,0)sample diluted due to high organic content,(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte,p)methylbenzene,(m)acetic acid ethenyl ester,(n)chloroethene,(o)dimethylbenzenes <br /> DHS Certification No 1644 /J Edward Hamilton,Lab Director <br />