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Curtis & Tompkins Labs GC/MS CONTINUING CALIBRATION REPORT FOR MSVOA04 to File: def02 Date Analyzed: 15-MAY-2000 Time Analyzed: 09 : 13 it Cal Date: 14-MAY-00 Meth: \\gcrossercrer\dd\chem\msvoa04. i\051500 .b\i4m826w.m Cpnound RF RF MinRF Actual Ouant IrD Max Flacrs Hexane COMPOUND NOT DETECTED 1-Chlorohexane COMPOUND NOT DETECTED 1,4-Dioxane COMPOUND NOT DETECTED Freon 12 0.3971 0 3876 0.0500 50.00 48 80 -2 30 Chloromethane 0 2976 0.2850 0 1000 50.00 47.89 -4 30 Vinyl Chloride 0.2641 0.2716 0.0500 50.00 51.41 3 20 Bromomethane 0.2441 0.1968 0.0500 50.00 44.78 -10 30 Chloroethane 0 1612 0.1464 0.0500 50.00 45.41 -9 30 Ethanol 0.0016 0.0012 0 0005 5000.00 3623 56 -28 40 Trichlorofluoromethane 0 4301 0.4205 0.0500 50.00 48.88 -2 30 Isopropanol 0 0109 0.0085 o ooso 500.00 392 18 -22 40 Acetone 0.0887 0.0805 0.0500 50.00 45.35 -9 40 Freon 113 0.2688 0.2788 0.0500 50 00 44.65 -11 30 1,1-Dichloroethene 0-2506 0.2685 0.0500 50.00 53.58 7 20 Methylene Chloride 0.3980 0.3712 0.0500 50.00 46.64 -7 30 Carbon Disulfide 1.0487 0.9603 0.0500 50.00 45 78 -8 30 MTBE 1.1908 1.0753 0 0500 50.00 45.15 -10 30 trans-1,2-Dxchloroethene 0.3665 0.3290 0.0500 50.00 44 89 -10 30 Vinyl Acetate 0.7630 0 7460 0 0500 50.00 48.89 -2 40 1,1-Dzchloroethane 0 6731 0.5929 0.1000 50.00 44 04 -12 30 • 2-Butanone 0.1732 0 1626 0 0500 50.00 46 95 -6 40 2,2-D3.chloropropane 0.5400 0.4939 0 0500 50.00 51.43 3 30 cis-1,2-Dzchloroethene 0 4229 0.3731 0 0500 50.00 44 12 -12 30 Chloroform 0.7079 0 6184 0 0500 50.00 43 68 -13 20 Bromochloromethane 0 2135 0.1890 0 0500 50.00 44.26 -11 30 Tetrahydrofuran 0 1029 0 0984 0 0050 500.00 478 24 -4 40 Dzbromofluoramethane 0.4725 0.4664 0.0500 50.00 49.36 -1 30 1,1,1-Trichloroethane 0 4983 0.4753 0 0500 50.00 47 70 -5 30 1,1-Dichloropropene 0.3432 0 3228 0.0500 50 00 47.04 -6 30 1,2-Dichloroethane-d4 0.3774 0.3738 0 0500 50.00 49 52 -1 30 Carbon Tetrachloride 0 3144 0 3089 0 0500 50 00 49.12 -2 30 1,2-Dichloroethane 0.3908 0.3471 0.0500 50 00 44 41 -11 30 Benzene 1.1673 1.0320 0 0500 50 00 44.20 -12 30 Trichloroethene 0 2852 0 2573 0.0500 50.00 45 12 -10 30 1,2-D3.chloropropane 0 3068 0.2722 0 0500 50.00 44 36 -11 20 Bromodichloromethane 0.4053 0.3645 0.0500 50 00 44 97 -10 30 Dibromomethane 0 1877 0 2009 0 0500 50 00 48 39 -3 30 2-Chloroethylvinylether 0 1290 0 1265 0 0500 50.00 49 02 -2 40 4-Methyl-2-Pentanone 0 2516 0 2395 0.0500 50.00 47 60 -5 40 cis-1,3-Dichloropropene 0 4774 0 4292 0 0500 50 00 44 96 -10 30 Toluene-d8 1 1173 1.1193 0 0500 50 00 50 09 0 30 Toluene 0 6828 0 6047 0.0500 50.00 44.29 -11 20 trans-1,3-Dxchloropropene 0 4134 0 3863 0.0500 50.00 46 72 -7 30 1,1,2-Trichloroethane 0 1595 0 1479 0 0500 50 00 46 38 -7 30 2-Hexanone 0.1919 0 1743 0 0500 50.00 45 41 -9 40 0 Page 1 of 2