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Curtis & Tompkins Labs <br /> GC/MS CONTINUING CALIBRATION REPORT FOR MSVOA02 <br /> a File: bef03 Date Analyzed: 15-MAY-2000 Time Analyzed: 09 :49 <br /> t Cal Date: 11-MAY-00 Meth: \\gcrosserver\dd\chem\msvoa02 . i\051500 .b\i2m826 .m <br /> Ca aund RF RF M1nRF Actual Quant %D Max Flacrs <br /> Dibromochloromethane 0 2551 0.2436 0 0500 50 00 47 74 -5 30 <br /> 1,2-Dibromoethane 0 1795 0 1671 0 0500 50 00 46 55 -7 30 <br /> Chlorobenzene 0 6348 0 5919 0 3000 50 00 46.62 -7 30 <br /> 1,1, 1,2-Tetrachloroethane 0 2208 0 2085 0 0500 50 00 47 21 -6 30 <br /> Fsthylbenzene 1 0156 0 9704 0.0500 50 00 47 77 -4 20 <br /> m,p-Xylenes 0 3706 0 3688 0 0500 100 00 99 51 0 30 <br /> o-Xylene 0 3614 0.3580 0 0500 50 00 49 54 -1 30 <br /> Styrene 0 6468 0 6307 0.0500 50 00 48.75 -2 30 <br /> Bromoform 0 1693 0.1614 0 1000 50 00 47 68 -5 30 <br /> Cyclohexanone 0 0127 0 0130 0 0050 500 00 510 29 2 40 <br /> Isopropylbenzene 1 9927 1 9372 0.0500 50 00 48.61 -3 30 <br /> 1,1,2,2-Tetrachloroethane 0 5651 0 5025 0 3000 50 00 44 46 -11 30 <br /> Bromofluorobenzene 1 0559 1.0138 0 0500 50 00 48 01 -4 30 <br /> 1,2,3-Trichloropropane 0 1294 0 1168 0.0500 50 00 45.13 -10 30 <br /> Bromobenzene 0 5522 0.5110 0 0500 50 00 46 27 -7 30 <br /> Propylbenzene 2 4351 2.4135 0 0500 50 00 49 56 -1 30 <br /> 2-Chlorotoluene 1 6190 1 5308 0 0500 50 00 47.28 -5 30 <br /> 1,3,5-Trimethylbenzene 1 4288 1 4813 0 0500 50 00 51 84 4 30 <br /> 4-Chlorotoluene 1 5023 1 4131 0 0500 50 00 47 03 -6 30 <br /> Cert-Butylbenzene 1 2757 1 3226 0 0500 50 00 51.84 4 30 <br /> • 1,2,4-Trimethylbenzene 1 3402 1 4029 0 0500 50 00 52 34 5 30 <br /> sec-Butylbenzene 2 0369 2 1261 0 0500 50 00 52 19 4 30 <br /> para-Isopropyl Toluene 1 4388 1 5987 0 0500 50 00 51.23 2 30 <br /> 1,3-Dichlorobenzene 0 9301 0 8977 0 0500 50 00 48 26 -3 30 <br /> 1,4-Dichlorobenzene 0 9398 0 9137 0 0500 50 00 48 61 -3 30 <br /> n-Butylbenzene 1 3533 1 5666 0 0500 50 00 53 .40 7 30 <br /> 1,2-Dichlorobenzene 0 8574 0 8248 0 0500 50 00 48 10 -4 30 <br /> 1,2-Dxbromo-3-Chloropropane 0 0768 0 0750 0 0500 50 00 48 82 -2 30 <br /> 1,2,4-Trzchlorobenzene 0 3166 0 4064 0 0500 50 00 57 95 16 30 <br /> Hexachlorobutadmene 0 2802 0 3013 0 0500 50 00 53 77 8 30 <br /> Naphthalene 0 5068 0 6183 0 0500 50 00 49 90 0 30 <br /> 1,2,3-Trichlorobenzene 0 3194 0 3715 0 0500 50 00 52 55 5 30 <br /> Internal Standard CgMound _ ICS Area CCS Area Diff ICS RT CCS RT Diff <br /> Pentafluorobenzene 797307 895799 +12 35 8 67 8.70 +0 02 <br /> 1,4-Difluorobenzene 1281597 1461315 +14 02 10.18 10 20 +0 02 <br /> Chlorobenzene-d5 1011663 1150836 +13 76 15.31 15 34 +0 03 <br /> 1,4-Dichlorobenzene-d4 484134 552094 +14 04 19 70 19 73 +0 03 <br /> • <br /> M=<5 ICS levels <br /> Page 2 of 2 <br />