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GeoAnalytical Laboratories, Inc. <br /> 2300 Maryann Dr. Turlock,CA 95380 Phone(209)669-0100 Fax(209)593-2212 <br /> email: la b.geo@att.net <br /> Report# Y2F2714 Date:07/11/12 <br /> San Joaquin County Environmental Health Date Recd:06/27/12 <br /> 1868 East Hazelton Ave <br /> Stockton,CA 95205 <br /> CERTIFICATE OF ANALYSIS <br /> Sampler: Thuy Tran <br /> Sample ID: North Trench Oil H2O Separator <br /> Lab ID Sample Date/Time RL Method Analyte Result Units Notes Started <br /> Y21`2714-01 6/26/2012 12:03 0.010 6020 Antimony 0.133 mg/L 7/2/12 08:10 <br /> 0.010 Arsenic 0.240 mg/L <br /> 0.100 Barium 5.41 mg/L <br /> 0.010 Beryllium ND mg/L <br /> 0.001 Cadmium 0.186 mg/L <br /> 0.010 Chromium 0.320 mg/L <br /> 0.010 Cobalt 0.047 mg/L <br /> 0.010 Copper 2.99 mg/L <br /> 0.010 Lead 0.517 mg/L <br /> 0.020 Molybdenum 0.298 mg/L <br /> 0.050 Nickel 0.310 mg/L <br /> 0.010 Selenium ND mg/L <br /> 0.020 Silver ND mg/L <br /> 0.010 Thallium ND mg/L <br /> 0.010 Vanadium 0.234 mg/L <br /> 0.050 Zinc 9.20 mg/L <br /> 0.001 6020A Mercury ND mg/L <br /> 0.1 9040B pH 3.2 Std.Units 6/27/12 16:08 <br /> 1.0 9214 Fluoride 38 mg/kg 7/2/12 10:03 <br /> Sample ID: Sludge from Trench Barrel <br /> Lab ID Sample Date/Time RL Method Analyte Result Units Notes Started <br /> Y21`2714-02 6/26/2012 12:03 0.5 6020 Antimony 6.3 mg/kg 7/3/12 08:43 <br /> 0.5 Arsenic 1.6 mg/kg <br /> 0.5 Barium 270 mg/kg <br /> 0.5 Beryllium ND mg/kg <br /> 0.5 Cadmium 2.0 mg/kg <br /> 0.5 Chromium 15 mg/kg <br /> 0.5 Cobalt 1.8 mg/kg <br /> 0.5 Copper 89 mg/kg <br /> 1.0 Lead 13 mg/kg <br /> 0.5 Molybdenum 22 mg/kg <br /> 0.5 Nickel 11 mg/kg <br /> 0.5 Selenium ND mg/kg <br /> 1.0 Silver ND mg/kg <br /> 0.5 Thallium ND mg/kg <br /> 0.5 Vanadium 8.9 mg/kg <br /> 0.5 Zinc 170 mg/kg <br /> 0.5 6020A Mercury ND mg/kg <br /> 0.1 9040B pH 5.6 Std.Units 6/27/12 16:10 <br /> 1.0 9214 Fluoride 170 mg/kg 7/2/12 10:03 <br /> Certification#2585 <br />