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n <br />MATRIX SPIRE SAMPLE EVALUATION REPORT <br />GC Semivolatiles <br />Client Lot # ---: E1F120269 Work Order #-•-: EERJ51AD-MS Matrix.........: SOLID <br />MS Lot -Sample #: E1F120269-007 EERJ51AE-MSD <br />Date Sampled...: 06/11/01 Date Received..: 06/12/01 10:00 MS Run #.......: 1164249 <br />Prep Date......: 06/13/01 Analysis Date..: 06/14/01 <br />Prep Batch #... : 1164461 Analysis Time..: 14:14 <br />Dilution Factor: 1 Analyst ID.....: 356074 Instrument ID..: G01 <br />PERCENT RECOVERY RPD <br />PARAMETER RECOVERY LIMITS RPD LIMITS METHOD <br />TPH (as Diesel) 266 a (60 - 130) SW846 8015B <br />368 a (60 - 130) 32 (0-35) SW846 8015B <br />Calculations are performed before rounding to avoid round -off errors in calculated results <br />Bold print denotes control parameters <br />a Spiked analyte recovery is outside stated control limits. <br />0(JO��� , <br />RECOVERY <br />LIMITS <br />(60 - 130) <br />(60 - 130) <br />PERCENT <br />SURROGATE <br />RECOVERY <br />Benzo(a)pyrene <br />86 <br />94 <br />NOTE (S) : <br />Calculations are performed before rounding to avoid round -off errors in calculated results <br />Bold print denotes control parameters <br />a Spiked analyte recovery is outside stated control limits. <br />0(JO��� , <br />RECOVERY <br />LIMITS <br />(60 - 130) <br />(60 - 130) <br />