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t <br />MATRIX SPIKE SAMPLE DATA REPORT <br />GC Semivolatiles <br />Client Lot #...: <br />E1F120269 <br />Work Order #...: EERJ51AD-MS Matrix <br />......... : SOLID <br />MS Lot -Sample : <br />EIF120269-007 <br />EERJ51AE-MSD <br />- <br />Date Sampled...: <br />06/11/01 <br />Date Received..: <br />06/12/01 <br />10:00 MS Run <br />#.......: 1164249 <br />Prep Date......: <br />06/13/01 <br />Analysis Date..: <br />06/14/01 <br />Prep Batch #...: <br />1164461 <br />Analysis Time..: <br />14:14 <br />Dilution Factor: <br />1 <br />Analyst ID.....: <br />356074 <br />Instrument ID..: G01 <br />SAMPLE SPIKE MEASRD <br />PERCENT <br />PARAMETER <br />AMOUNT AMT AMOUNT <br />UNITS <br />RECOVERY RPD <br />METHOD <br />TPH (as Diesel) <br />ND <br />250 664 <br />mg/kg <br />266 a <br />SW846 8015B <br />ND <br />250 919 <br />mg/kg <br />368 a 32 <br />SW846 8015B <br />SURROGATE <br />Benzo(a)pyrene <br />NOTE(S): <br />PERCENT RECOVERY <br />RECOVERY LIMITS <br />86 (60 - 130) <br />94 (60 - 130) <br />Calculations are performed before rounding to avoid round -off errors in calculated results. <br />Bold print denotes control parameters <br />a Spiked analyte recovery is outside stated control limits. <br />E <br />000 <br />