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11/16/98 MON 17:24 FAX 2094671118 <br />1 0 <br />ffli � t <br />11 <br />I 10 Second Avenue South, #D7, Pacheco, CA 94553-5560 <br />McCAAOBELL ANALYTICAL INC. I Telephone: 925-798-1620 Pax:925-798-1622 <br />Advanced GredEnvironniental Client Project 111S.J. County Corporate <br />Date Sampled: 11104198 <br />Date Received: 11/05/98 <br />4005 North Wilson Way Yard <br />Date Ex d: 11/05/98 <br />Stockton, CA 95205 Client Contact: Tim Cuellar <br />Date Analyzed: 11/06/98 <br />Client P.O: <br />Lead* <br />EPA analytical metbods 6010/200.7,239,r <br />Lab ID <br />Client ID <br />Matrix <br />on <br />Lead* <br />-- —Recovery <br />®� <br />LU me <br />98160 <br />TKI-West <br />S <br />TTLC <br />10 <br />98 <br />98161 <br />TKI-Middle <br />S <br />TTLC <br />8.4 <br />99 <br />98162 <br />TKI-East <br />S <br />TTLC <br />8.4 <br />100 <br />98165 <br />Pipe I <br />S <br />TTLC <br />5.5 <br />101 <br />98166 <br />Pipe 2 <br />S <br />TTLC <br />7.0 <br />98 <br />98170 <br />SPBI-2 <br />S <br />TTLC <br />5.3 <br />99 <br />98171 <br />SPB3-4 <br />S <br />TTLC <br />4.6 <br />96 <br />99172 <br />SPBS-6 <br />S <br />TTLC <br />5.4 <br />101 <br />S TTLC <br />3.0 M&g <br />Reporting limit unless otherwise <br />stated; ND means not detected above W TTLC <br />0-005 MSIL <br />the reporting limit <br />— STLCTCLP <br />U Mg/L <br />soil and sludge samples am reported in mgft, wipe samples in ug/wipe, and water samples and all STLC t SPLP TCLP extracts in mg/L <br />''Lead is analysed using EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br />samples <br />EPA extraction methods 131 I(TCLF), 3010020(waterTTLC), 3040(organic matricesTTLC), 3050(solids,TTLC); STLC - CA Tide 22 <br />surrogate diluted out of range; N/A means surropte not applicable to this analysis <br />reporting limit raised due matrix interkrence <br />i) liquid sample that contains greater than –2 vol. % sediment; this sedirnent is <br />witracted with the liquid, in accordance with EPA <br />methodologies and can significantly effect reported metal concentrations. <br />DHS Certification No. 1644 <br />Edward Hamilton, Lab Director <br />M <br />