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11/16/98 MON 17:22 FAX 2094671118 AGE-STOCKTON 191005 <br />• 10 <br />110 Second Avenue South, 07, Pacheco, CA 94553-5560 <br />14 1 MCCAWBELL ANALYTICAL INC. Telephone: 925-798-1620 Fax: 925-798-1622 <br />httn://www.mocamn e1b l.cnm E-mail: main@rnccamphell.com <br />Advanced GeoEnvimamental Client Project ID: S.J. County Corporate Date Sampled: 11/04/98 <br />4005 North Wilson Way Yard Date Received: 11/05/98 <br />Stockton, CA 95205 Client Contact: Tim Cuellar Date Extracted: 11/06/98 <br />Clicnt P.O: Date Analyzed: 11/06-11/08/98 <br />EPA method 8260 modified <br />Lab ID <br />98160 <br />98161 <br />98162 <br />98165 <br />Reporting <br />Limit <br />Client ID <br />TKI- West T KI -Middle <br />TK1 East <br />Pipe I <br />Matrix <br />S <br />S <br />S <br />S <br />S <br />W <br />Compound <br />Concentration* <br />ug/kg <br />ug/L <br />Di -isopropyl Ether (DIPS) <br />ND <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />Ethyl tert-Butyl Ether MBE) <br />ND <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />Methyl-tert Butyl Ether (MTBE) <br />ND <br />ND <br />43 <br />210 <br />5.0 <br />1.0 <br />tert Amyl Methyl Ether (TAME) <br />ND <br />ND <br />ND <br />ND <br />5.0 <br />1.0 <br />tert-Butanol <br />ND <br />ND <br />ND <br />ND <br />25 <br />1 5.0 <br />Surrogate Recoveries (%)' <br />Di wwfluoromethme 92 92 92 100 <br />Comments: F_ <br />e water samples ane reported in ugd , soil and sludge samples in ug/kg, wipes in ughApe and all TCLP / STLC / SPLP extracts in ug/L <br />ND means not detected above the reporting limit; N/A means surrogate not applicable to this analysis <br />(h) lighter then water immiscible sheen is present; (1) liquid sample that contains greater than —5 vol. % sediment; 0) sample diluted due to <br />high organic content <br />DHS Certification No. 1644 // Edward Hamilton, Lab Director <br />