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41� Sequoia <br />080 Chesapeake Drive <br />Redwood City, CA 9406*415) 364-9600 <br />FAX (415) 364-9233 <br />VAW Analytical <br />404 N. Wiget Lane <br />819 Striker Avenue, Suite 8 <br />Walnut Creek, CA 94598 (510) 988-9600 <br />Sacramento, CA 95834 (916) 921-9600 <br />FAX (510) 988-9673 <br />FAX (916) 921-0100 <br />3164 Gold Camp Dr., Suite 200 Matrix: Soil <br />Rancho Cordova, CA 95670 <br />Attention: Eric Holm OC Sample Group 5080401-403 Reported: Aug 15, 1 <br />QUALITY CONTROL DATA REPORT <br />ANALYTE Ethyl- 1,1-Dichloro- Trichloro- <br />Benzene Toluene Benzene Xylenes ethane ethene Chlorobenzene <br />Method: <br />EPA 8020 <br />EPA 8020 <br />EPA 8020 <br />EPA 8020 <br />EPA 8010 <br />EPA 8010 <br />EPA 8010 <br />Analyst: <br />C. Chapman <br />C. Chapman <br />C. Chapman <br />C. Chapman <br />K. Pocan <br />K. Pocan <br />K. Pocan <br />Concentration <br />Spiked: <br />0.20 mg/kg <br />0.20 mg/kg <br />0.20 mg/kg <br />0.60 mg/kg <br />10 ug/L <br />10 ug/L <br />10 ug/L <br />LCS Batch#: <br />LCS081095 <br />LCS081095 <br />LCS081095 <br />LCS081095 <br />LCS081195 <br />LCS081195 <br />LCS081195 <br />Date Prepared: <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/11/95 <br />8/11/95 <br />8/11/95 <br />Date Analyzed: <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/11/95 <br />8/11/95 <br />8/11/95 <br />Instrument I.D.#: <br />GCHP-1 <br />GCHP-1 <br />GCHP-1 <br />GCHP-1 <br />GCHP-5 <br />GCHP-5 <br />GCHP-5 <br />LCS % <br />Recovery: <br />93 <br />94 <br />93 <br />93 <br />92 <br />95 <br />70 <br />Control Limits: <br />75-125 <br />75-125 <br />75-125 <br />75-125 <br />70-130 <br />70-130 <br />70-130 <br />MS/MSD <br />Batch #: <br />5080357 <br />5080357 <br />5080357 <br />5080357 <br />5080011 <br />5080011 <br />5080011 <br />Date Prepared: <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />Date Analyzed: <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />8/10/95 <br />Instrument I.D.#: <br />GCHP-1 <br />GCHP-1 <br />GCHP-1 <br />GCHP-1 <br />GCHP-5 <br />GCHP-5 <br />GCHP-5 <br />Matrix Spike <br />% Recovery: <br />98 <br />97 <br />100 <br />99 <br />84 <br />100 <br />117 <br />Matrix Spike <br />Duplicate % <br />Recovery: <br />98 <br />99 <br />102 <br />102 <br />71 <br />83 <br />87 <br />Relative % <br />Difference: <br />0.0 <br />2.0 <br />2.0 <br />3.0 <br />17 <br />19 <br />29 <br />SEQUOIA ANALYTICAL <br />Linda C. Schneider <br />Project Manager <br />Please Note: <br />The LCS is a control sample of known, interferent free matrix that is analyzed using the same reagents, <br />preparation and analytical methods employed for the samples. The LCS % recovery data is used for <br />validation of sample batch results. Due to matrix effects, the QC limits for MS/MSD's are advisory only <br />and are not used to accept or reject batch results. <br />0 <br />5080401.DLT <7> <br />