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M*fum VERIFICATION LABORATORY AYSIS <br /> TANK TANK TPH-G TPH-D BTX&E CL HC TOTAL METALS PCB <br /> # CONTENTS 8015 8015 8020 8010 LEAD ICRP/ 8270 <br /> 8260 8260 8260 8240 7420 AES or 8080 <br /> 7421 AA <br /> LEADED <br /> GAS X X X <br /> ® UNL GAS X X <br /> DIESEL X X <br /> KEROSENE X X <br /> UNK FUEL X X X X <br /> PROD. OIL X X <br /> CHLOR <br /> SOLVEN'T'S X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTE <br /> USED OIL X X X X X X <br /> All analyses methods are designated EPA methods described in EPA SW 846,Third Edition. Those methods not found <br /> in SW 846,are specifically noted below. Refer to the"SWRCB LUFT Field Manual",Appendix A-20,Table 3-5 for <br /> detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of USTs"for the waste and motor oil detection limits. <br /> Detection Limits that remain below the MCI., STLC or Allowable Limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY- <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon,Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> BTX& E Benzene,Toluene,Xylene &Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/USD 8010, GC/MS 8240 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> EDB Ethylene dibromide(DHS-AB 1803), G IMS 8240 (DHS-LUFT) <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium III and VI,Lead, Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene,benzene-free solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column may be used as a "fust cut"with "dirty"samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed <br /> For Drinking water sources,EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated. <br /> EH 23 048 (Revised 7/10/92) Page 8 <br />