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(5) <br />Sample <br />Result (ug/kg) <br />ID <br />Compound <br />MB <br />methyl Cert -butyl ether (MTBE) <br />MB <br />di -isopropyl ether (DIPE) <br />MB <br />ethyl tert-butyl ether (ETBE) <br />MB <br />tert-amyl methyl ether (TAME) <br />Surrogate (ug/kg) <br />Result (ug/kg) <br />% Recovery <br />Acceptance Range (%) <br />dibromofluoromethane (125) <br />133 <br />106 <br />70-130 <br />Sample Sample <br />Spike <br />ID <br />Compound <br />1824 CMS <br />methyl tent -butyl ether (MTBE) <br />CMS <br />di -isopropyl ether (DIPE) <br />CMS <br />ethyl tent -butyl ether (ETBE) <br />CMS <br />tert-amyl methyl ether (TAME) <br />Result <br />Spike <br />% <br />(u /kq) <br />Level <br />Recv. <br />97.3 <br />100 <br />97.3 <br />92.5 <br />100 <br />92.5 <br />90.4 <br />97.9 <br />92.3 <br />172 <br />181 <br />95.0 <br />Surrogate (ug/kg) <br />Result (ug/kg) <br />% Recovery <br />Acceptance Range (%) <br />dibromofluoromethane (104) <br />112 <br />108 <br />70-130 <br />Sample Sample <br />ID <br />1824 CMSD <br />CMSD <br />CMSD <br />CMSD <br />methyl tert-butyl ether (MTBE) <br />di -isopropyl ether (DIPE) <br />ethyl tert-butyl ether (ETBE) <br />tert-amyl methyl ether (TAME) <br />Result <br />Spike <br />% <br />Acceptance Range (%) <br />ug/kg) <br />Level <br />Recv. <br />RPD <br />94.6 <br />100 <br />94.6 <br />2.8 <br />93.1 <br />100 <br />93.1 <br />0.65 <br />91.5 <br />97.9 <br />93.5 <br />1.2 <br />172 <br />181 <br />95.0 <br />0.0 <br />Surrogate (ug/kg) <br />Result (ug/kg) <br />% Recovery <br />Acceptance Range (%) <br />dibromofluoromethane (104) <br />116 <br />111 <br />70-130 <br />MB = Method Blank; LCS = Laboratory Control Sample; CMS = Client Matrix Spike; CMSD = Client Matrix Spike Duplicate <br />NS = Not Spiked; OR = Over Calibration Range <br />Page 38 of 38 <br />CA Lab Accreditation #: 2118 / 1-2303 <br />