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Clayton <br />LABORATORY <br />SERVICES <br />Page 7 of 10 <br />Method <br />Detection <br />Concentration Limit <br />Analyte CAS # (mg/kg) (mg/kg) <br />Base/Neutral Extractables (Continued) <br />2-Nitroaniline <br />Analytical Results <br />ND <br />1 <br />3-Nitroaniline <br />for <br />ND <br />1 <br />4-Nitroaniline <br />Analytical Sciences <br />ND <br />1 <br />Nitrobenzene <br />Client Reference: WT98001 <br />(8042301) <br />0.2 <br />N-Nitrosodiphenylamine <br />Clayton Project No. 98043.53 <br />ND <br />0.2 <br />Sample Identification: <br />WOSP (A&B)(1823) <br />Date Sampled: <br />04/23/98 <br />Lab Number: <br />9804353-02A <br />Date Received: <br />04/27/98 <br />Sample Matrix/Media: <br />SOIL <br />Date Extracted: <br />05/01/98 <br />Extraction Method: <br />EPA 3550 <br />Date Analyzed: <br />05/05/98 <br />Method Reference: <br />EPA 8270B <br />Analyst: <br />ASC <br />Method <br />Detection <br />Concentration Limit <br />Analyte CAS # (mg/kg) (mg/kg) <br />Base/Neutral Extractables (Continued) <br />2-Nitroaniline <br />88-74-4 <br />ND <br />1 <br />3-Nitroaniline <br />99-09-2 <br />ND <br />1 <br />4-Nitroaniline <br />100-01-6 <br />ND <br />1 <br />Nitrobenzene <br />98-95-3 <br />ND <br />0.2 <br />N-Nitrosodiphenylamine <br />86-30-6 <br />ND <br />0.2 <br />N-Nitrosodi-n-propylamine <br />621-64-7 <br />ND <br />0.2 <br />Phenanthrene <br />85-01-8 <br />ND <br />0.2 <br />Pyrene <br />129-00-0 <br />ND <br />0.2 <br />1,2,4-Trichlorobenzene <br />120-82-1 <br />ND <br />0.2 <br />Surrogates <br />Recovery (%) QC Limits M <br />2-Fluorobiphenyl <br />321-60-8 <br />88 <br />30 <br />- 115 <br />2-Fluorophenol <br />367-12-4 <br />66 <br />25 <br />- 121 <br />Nitrobenzene -d5 <br />4165-60-0 <br />79 <br />23 <br />- 120 <br />Phenol -d5 <br />13127-88-3 <br />78 <br />24 <br />- 113 <br />Terphenyl-d14 <br />98904-43-9 <br />94 <br />-18 <br />- 137 <br />2,4,6-Tribromophenol <br />118-79-6 <br />72 <br />19 <br />- 122 <br />ND: Not detected at or above limit of detection <br />--. Information not available or not applicable <br />Results are reported on a wet -weight basis, as received. <br />