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MIPWM VERIFICA'T'ION I.ABOItATORY ANOVSIS <br />TANK <br /># <br />TANK <br />CONTENTS <br />TPII-G <br />8015 <br />8260 <br />TPII-D <br />8015 <br />8260 <br />BTX & E <br />8(0) <br />8260 <br />CL I IC <br />8010 <br />8240 <br />TOTAL <br />LEAD <br />7420 <br />747.1 <br />EDB <br />8240 <br />METALS <br />ICAP/ <br />AES or <br />AA <br />FCB <br />8270 <br />8080 <br />EDB <br />LEADED <br />GAS <br />X <br />Gas Chromatography, Flame Ionization Detection <br />X <br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Abs6rption <br />X <br />X <br />PCB <br />Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br />Method 3050 <br />UNL GAS <br />X <br />Sox.hlet sample preparation <br />x <br />Sonication sample preparation, extraction method <br />Method 5030 <br />Purge and trap sample preparation <br />QA/QC <br />Quality Assurance/Quality Conti0l <br />DIESEL <br />X <br />X <br />KEROSENE <br />X <br />X <br />UNK FUEL <br />X <br />X <br />X <br />X <br />x <br />LO <br />CHLOR. <br />SOLVENTS <br />X <br />Y <br />NONCI ILOR <br />SOLVEN75 <br />X <br />X <br />X <br />WAS <br />All analyses methods are designated EPA methods described in EPA SW 846, Third Edition. Those methods not found <br />In SW 846, are specifically noted below. Refer to the "SWRCB LUFC Field Manual", Appendix A-20, Table 3-5 for <br />detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br />Initial Evaluation and Investigation of US'I's" for the waste and motor oil detection limits. <br />Detection Limits that remain below the MCI, STLC or Allowable Limit or the contaminant hr question will he accepted, <br />however laboratory shall utilize the most conservative method. <br />LABORATORY ANALYSES TERMINOLOGY: <br />'ITII-G <br />Total Petroleum hydrocarbon, Gasoline, GCyFID (5030) 8015 mod or GC NIS 8260 <br />TPIi-D <br />Total Petroleum Hydrocarbon, Dicscl, GC/FID (3550), 8015 mod or GC MS 8260 <br />BTX & E <br />Benzene, Toluene, Xylene & Ethyl Benzene., GCJPID 8020 or GC/MS 8260 <br />CL HC <br />Chlorinated hydrocarbon, GC/IISD 8010, GClMS 8240 <br />TOTAL LEAD <br />Total lead, AA 7420, AA 7421 or ICP -ACS W10 <br />EDB <br />Ethylene dibromide (DIIS-AB 1803), GC/NIS 8240 (DI iS-LUFT) <br />GC -FID <br />Gas Chromatography, Flame Ionization Detection <br />ICAP or AA <br />Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Abs6rption <br />Spectrometry 7(()O. Metals: Cndnrhrm, C1rrt1rniurn III and VI, Leant, Zinc mrd Nickel. <br />PCB <br />Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br />Method 3050 <br />Acid digestion <br />Method 3540 <br />Sox.hlet sample preparation <br />Method 3550 <br />Sonication sample preparation, extraction method <br />Method 5030 <br />Purge and trap sample preparation <br />QA/QC <br />Quality Assurance/Quality Conti0l <br />Notes: To avoid false positive detection of benzene, benzene -free solvents are to be used. Fused capillary columns are <br />preferred to packed columns; a packed column may be used as a "first cut" with "dirty" samples or once the hydrocarbons <br />have been characterized and proper QA/AC is followed. <br />For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br />series because the deteclion limits are lower and the QA/QC fs better. Samples exhibiting any level of heavy metal <br />contamination may require further analysis. PHS-EhD recommends holding these samples until disposal Is indicated. <br />Ell 23 048 (Revised 7/10/92) Page 8 <br />0 0 <br />