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cCampbell Analytical, Inc.I 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Web: www.mccampbell.com E-mail: main(bmccampbell.com <br />W.O. Sample Matrix: Water <br />QC Matrix: Water BatchlD: 40019 WorkOrder 0812110 <br />EPA Method SW8270C <br />Extraction SW3510C <br />Spiked Sample ID: <br />NIA <br />Analyte <br />Sample <br />pg/L <br />Spiked <br />pg/L <br />MS <br />% Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rec. <br />LCSD <br />% Rec. <br />LCS-LCSD Acceptance <br />% RPD MS / MSD RPD <br />Criteria (%) <br />LCS/LCSD <br />RPD <br />Acenaphthene <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />62.1 <br />59.2 <br />4.85 <br />N/A <br />N/A <br />30 -130 <br />20 <br />4-Chloro-3-methylphenol <br />N/A <br />100 <br />N/A <br />N/A <br />N/A <br />72.9 <br />74.7 <br />2.42 <br />N/A <br />N/A <br />30-130 <br />20 <br />2 -Chlorophenol <br />N/A <br />100 <br />N/A <br />N/A <br />N/A <br />73.8 <br />71.6 <br />2.96 <br />N/A <br />N/A <br />30-130 <br />20 <br />1,4 -Dichlorobenzene <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />62.3 <br />58.6 <br />6.07 <br />N/A <br />N/A <br />30- 130 <br />20 <br />2,4-Dinitrotoluene <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />66 <br />64.1 <br />2.97 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />4-Nitrophenol <br />N/A <br />100 <br />N/A <br />N/A <br />N/A <br />77.3 <br />75.9 <br />1.89 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />N-Nitrosodi-n-propylamine <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />78 <br />84.2 <br />7.61 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />Pentachlorophenol <br />N/A <br />100 <br />N/A <br />N/A <br />N/A <br />45.2 <br />43 <br />4.95 <br />N/A <br />N/A <br />30-130 <br />20 <br />Phenol <br />N/A <br />100 <br />N/A <br />N/A <br />N/A <br />66.4 <br />67.6 <br />1.79 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />Pyrene <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />69.1 <br />65.5 <br />5.27 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />1,2,4-Trichlorobenzene <br />N/A <br />50 <br />N/A <br />N/A <br />N/A <br />62.5 <br />60.7 <br />2.91 <br />N/A <br />N/A <br />30 -130 <br />20 <br />%SSI: <br />N/A <br />5000 <br />N/A <br />N/A <br />N/A <br />64 <br />65 <br />2.55 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />%SS2: <br />N/A <br />5000 <br />N/A <br />N/A <br />N/A <br />66 <br />66 <br />0 <br />N/A <br />N/A <br />30-130 <br />20 <br />%SS3: <br />N/A <br />5000 <br />N/A <br />N/A <br />N/A <br />66 <br />66 <br />0 <br />N/A <br />N/A <br />30-130 <br />20 <br />%SS4: <br />N/A <br />5000 <br />N/A <br />N/A <br />N/A <br />60 <br />58 <br />3.51 <br />N/A <br />N/A <br />30 - 130 <br />20 <br />%SS5: <br />N/A <br />5000 <br />N/A <br />N/A <br />N/A <br />86 <br />83 <br />3.73 <br />N/A <br />N/A <br />30-130 <br />20 <br />%SS6: <br />N/A <br />1 5000 <br />N/A <br />N/A <br />N/A <br />1 68 <br />1 66 <br />1 3.10 <br />N/A <br />N/A <br />30- 130 <br />20 <br />All target compounds in the Method <br />NONE <br />Blank of this extraction batch were ND less than the <br />method RL with the following exceptions: <br />BATCH 40019 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br />08 12110-00 1C 12/02/08 12/03/08 12/05/08 8:07 AM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100 " (MS -Sample) / (Amount Spiked); RPD = 100 . (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND <br />contains significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />extraction solvents such as methylene chloride and acetone <br />DHS ELAP Certification 1644 <br />in the method blank at low levels. <br />QA/QC Officer <br />