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cCampbell Analytical+ Inc. 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Web: www.mccainpbell.com E-mail: main(&mccampbell.com <br />"When Oualitv Counts" I Telephone: 877-252-9262 Fax: 925-252-9269 <br />Test Method: <br />Ignitability <br />Matrix: W <br />WorkOrder: 0812110 <br />Method Name: SW1010 <br />Units t °C <br />BatchlD: 40067 <br />Lab ID <br />Sample <br />DF Dup / Ser. Dil. <br />DF % RPD <br />Acceptance Criteria (%) <br />0812110-OOIF <br />>100 °C <br />1 >100 °C <br />1 N/A <br /><15 <br />Lab ID <br />Date Sampled Date Extracted <br />BATCH 40067 SUMMARY <br />Date Analyzed Lab ID <br />Date Sampled Date Extracted Date Analyzed <br />0812110-OOIF <br />12/02/08 12/10/08 <br />12/10/08 1:10 PM <br />Test Method: <br />Reactive Cyanide <br />Matrix: W <br />WorkOrder: 0812110 <br />Method Name: SWchpt7_CN <br />Units pos/neg <br />BatchlD: 40068 <br />Lab ID <br />Sample <br />DF Dup / Ser. Dil. <br />DF % RPD <br />Acceptance Criteria (%) <br />0812110-OOIF <br />neg <br />1 neg <br />1 N/A <br />N/A <br />Lab ID <br />Date Sampled Date Extracted <br />BATCH 40068 SUMMARY <br />Date Analyzed Lab ID <br />Date Sampled Date Extracted Date Analyzed <br />0812110-OOIF <br />12/02/08 12/10/08 <br />12/10/08 4:10 PM 10812110-00 1F <br />12/02/08 <br />12/10/08 12/10/08 4:10 PM <br />Test Method: <br />Reactive Sulfide <br />Matrix: W <br />WorkOrder: 0812110 <br />Method Name: SWchpt7_S <br />Units pos/neg <br />BatchlD: 40068 <br />Lab ID <br />Sample <br />DF Dup / Ser. Dil. <br />DF % RPD <br />Acceptance Criteria (%) <br />0812110-001F <br />nig <br />1 neg <br />1 N/A <br />N/A <br />Lab ID <br />Date Sampled Date Extracted <br />BATCH 40068 SUMMARY <br />Date Analyzed Lab ID <br />Date Sampled Date Extracted Date Analyzed <br />0812110-001F <br />12/02/08 12/10/08 <br />12/10/08 4:10 PM 0812110-001F <br />12/02/08 <br />12/10/08 12/10/08 4:10 PM <br />Dup = Duplicate; Ser. Dil. = Serial Dilution; MS = Matrix Spike; RD = Relative Difference; RPD = Relative Percent Deviation. <br />Precision = Absolute Value (Sample - Duplicate) <br />RPD = 100 ' (Sample - Duplicate) / [(Sample + Duplicate) / 21 <br />%RPD is calculated using results of up to 10 significant figures, however the reported results are rounded to 2 or 3 significant figures. Therefore there may be a slight <br />discrepancy between the %RPD displayed above and %RPD calculated using the reported results. MAI considers %RPD based upon more significant figures to be more <br />accurate. <br />DHS ELAP Certification 1644 'IF-- QA/QC Officer <br />