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0 0 <br />cCampbell Analytical,Inc. 1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Web: www.mccampbell.com E-mail: main(rbmccampbell.com <br />"When Oualitv Counts" Telephone: 877-252-9262 Fax: 925-252-9269 <br />QC SUMMARY REPORT FOR SW8015B <br />W.O. Sample Matrix: Water CIC Matrix: Water BatchlD: 40061 WorkOrder 0812110 <br />EPA Method SW8015B <br />Extraction SW3510C <br />Spiked Sample ID: NIA <br />Analyte <br />Sample Spiked IVIS <br />pg/L pg/L % Rec. <br />MSD <br />% Rec. <br />MS -MSD <br />% RPD <br />LCS <br />% Rec. <br />LCSD <br />% Rec. <br />LCS-LCSD Acceptance Criteria (%) <br />% RPD MS / MSD RPD LCS/LCSD RPD <br />TPH-Diesel (C10 -C23) <br />N/A 1000 N/A <br />N/A <br />N/A <br />90.2 <br />97.9 <br />8.18 N/A N/A 70- 130 30 <br />%SS: <br />N/A 2500 N/A <br />N/A <br />N/A <br />101 <br />1 98 <br />2.55 1 N/A N/A 70 - 130 30 <br />All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: <br />NONE <br />BATCH 40061 SUMMARY <br />Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed <br />08 1 2 1 10-00 1 A 12/02/08 12/03/08 12/04/08 6:21 AM <br />MS = Matrix Spike; MSD = Matrix Spike Duplicate; LCS = Laboratory Control Sample; LCSD = Laboratory Control Sample Duplicate; RPD = Relative Percent Deviation. <br />% Recovery = 100 ` (MS -Sample) / (Amount Spiked); RPD = 100 ` (MS - MSD) / ((MS + MSD) / 2). <br />MS / MSD spike recoveries and / or %RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons: a) the sample is inhomogenous AND <br />contains significant concentrations of analyte relative to the amount spiked, or b) the spiked sample's matrix interferes with the spike recovery. <br />N/A = not enough sample to perform matrix spike and matrix spike duplicate. <br />NR = analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. <br />DHS FLAP Certification 1644 QA/QC Officer <br />