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Analyte: <br />1,1-Dichloro- <br />Trichloro- <br />Chloro- <br />Sample Conc.: <br />ethane <br />ethene <br />benzene <br />QC Batch#: <br />SP061698 <br />SP061698 <br />SP061698 <br />Analyzed Date: <br />8010EXA <br />8010EXA <br />8010EXA <br />Analy. Method: <br />EPA 8010 <br />EPA 8010 <br />EPA 8010 <br />Prep. Method: <br />EPA 5030 <br />EPA 5030 <br />EPA 5030 <br />Analyst: <br />N. Nelson <br />N. Nelson <br />N. Nelson <br />MS/MSD #: <br />8060193 <br />8060193 <br />8060193 <br />Sample Conc.: <br />N.D. <br />N.D. <br />N.D. <br />Prepared Date: <br />6/16/98 <br />6/16/98 <br />6/16/98 <br />Analyzed Date: <br />6/16/98 <br />6/16/98 <br />6/16/98 <br />Instrument I.D.#: <br />HP -6 <br />HP -6 <br />HP -6 <br />Conc. Spiked: <br />200pg/Kg <br />200Ng/Kg <br />2001jg/Kg <br />Result: <br />190 <br />190 <br />160 <br />MS % Recovery: <br />95 <br />95 <br />80 <br />Dup. Result: <br />200 <br />200 <br />180 <br />MSD % ecov.: <br />100 <br />100 <br />90 <br />RPD: <br />5.1 <br />5.1 <br />12 <br />RPD Limit: <br />0-25 <br />0-25 <br />0-25 <br />LCS #: <br />LCS061698 <br />LCS061698 <br />LCS061698 <br />Prepared Date: <br />6/16/98 <br />6/16/98 <br />6/16/98 <br />Analyzed Date: <br />6/16/98 <br />6/16/98 <br />6/16/98 <br />Instrument I.D.#: <br />HP -6 <br />HP -6 <br />HP -6 <br />Conc. Spiked: <br />200Ng/Kg <br />200pg/Kg <br />200pg/Kg <br />LCS Result: <br />190 <br />190 <br />170 <br />LCS % Recov.: <br />95 <br />95 <br />85 <br />LCS 65-135 70-130 70-130 <br />Control Limits <br />SEQUOIA ANALYTICAL, #1271 <br />I <br />�%ProjecMa ger <br />Please Note: <br />The LCS is a control sample of known, interferent -free matrix that is analyzed using the same reagents, <br />preparation, and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br />fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br />the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br />interference, the LCS recovery is to be used to validate the batch. <br />** M =Matrix pike, MSD= MS Duplicate, RPD= Relative % Difference <br />8061676.GET <2> <br />