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ALIFORNIA LABORATORY SERVICES <br /> Page 7 of 8 10/09/09 14:52 <br /> Padre Associates,Inc. Project: Kaiser-Manteca <br /> 3020 Explorer Dr.,Suite 5 Project Number: [none] CLS Work Order#:C&I0302 <br /> Sacramento,CA 95827 Project Manager: Alan Churchill COC#: 107798 <br /> Volatile Organic Compounds by EPA Method 8260B-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result °/uREC Limits RPD Limit Notes <br /> Batch CS07684-EPA 5030 Soft NIS <br /> Blank(CS07684-BLKI) Prepared&Analyzed: 10/09/09 <br /> 1,2,4-Trimethylbenzene ND 5.0 µg/kg <br /> Vinyl chloride ND 10 " <br /> Xylenes(total) ND 10 " <br /> Di-isopropyl ether ND 5.0 " <br /> Ethyl tert-butyl ether ND 5.0 " <br /> tert-Amyl methyl ether ND 5.0 " <br /> tert-Butyl alcohol ND 50 " <br /> Surrogate:l.2-Dichloroethane-d4 71.8 50.0 144 50-125 QS-HI <br /> Surrogate:Toluene-d8 50.7 50.0 101 62-125 <br /> Surrogate:4-Bromofluorobenzene 54.6 50.0 109 50-128 <br /> LCS(CS07684-BS1) Prepared&Analyzed: 10/09/09 <br /> Benzene 21.1 5.0 µg/kg 20.0 105 64-135 <br /> Chlorobenzene 21.2 5.0 20.0 106 67-133 <br /> 1,1-Dichloroethene 19.5 5.0 20.0 98 53-137 <br /> Toluene 22.5 5.0 20.0 113 61-138 <br /> Trichloroethene 20.9 5.0 20.0 104 64-130 <br /> Surrogate:1,2-Dichloroethane-d4 44.0 50.0 88 50-125 <br /> Surrogate:Toluene-d8 50.8 50.0 102 62-125 <br /> Surrogate:4-Bromofluorobenzene 49.6 50.0 99 50-128 <br /> LCS Dup(CS07684-BSDI) Prepared&Analyzed: 10/09/09 <br /> Benzene 16.6 5.0 gg/kg 20.0 83 64-135 24 30 <br /> Chlorobenzene 15.9 5.0 20.0 80 67-133 29 30 <br /> 1,1-Dichloroethene 15.7 5.0 20.0 78 53-137 22 30 <br /> Toluene 17.6 5.0 20.0 88 61-138 25 30 <br /> Trichloroethene 16.6 5.0 20.0 83 64-130 23 30 <br /> Surrogate:1,2-Dichloroethane-d4 44.9 50.0 90 50-125 <br /> Surrogate:Toluene-d8 53.2 50.0 106 62-125 <br /> Surrogate:4-Bromofluorobenzene 47.9 50.0 96 50-128 <br /> CA DOHS FLAP Accreditation/Registration Number 1233 <br /> 3249 Fitzgerald Road Rancho Cordova,CA 95742 www.californialab.com 916-638-7301 Fax:916-638-4510 <br />