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03/07/2005 16:17 2094683433 E MINIMUM VERIFICATION LABORATORY ANALYSIS specifically noted below. Refer to the "SMCB LUFT Field Martual"t Appendix D (B). Table 3-5 on page A7.0 for ininimim, d"et ectim jjpp�,. for Motor V911iCle fuel (gasoline and diesel). Refer to, -Ttj-Re&nal Board Suff Reconarnandations, for bitial Evaluation and kvesogat:Wn of'Ugrs" fbr the waste and motor oil minimut detection limits. Detechon Louts that remain beWw the MCL, STLC or Allowable Limit of the contandnant in question will be aceepted, however laboratory shall utilize the most conservative method. VA-WIRUS) TPH-G Total Petmk-umHydrocarbo�Gasffinc,CC/FD (5030)gOtSnlodorGCWS9260 TpH-D Total Pmoleum HydrombM Diesel, GCTID (3550), 9015 mod or GAS SM 8TX & EBcnzeno, Toluene, Xylene & EtW Be=ene, GOPID 8020 or GCWS 9260 CLK ChWnaWH)*wAftnGCIEWSOI OWMS92400r$260 TOTAL LEAD TOW lead, AA 7420, AA 7421 or 14CP-AES 6010 OXYGENATES UrMEETRE, TAME, D1PF,&TBA GOMS 8260 (For MM=vgL2WXyou =yuse 80M METALS ICAP or AA Inductively Coupled Plasina Atoniic Emission Spedroofty 6010 or Atomic Absorption Spec"itfty 7000 Metals: CatWvn16 Chromium M and V1, Lead, Efte and NWceL PC8 Polyctlorbiated DiphcnyK GOMS 9270 or SM GC -F rD Gas Chromatography, Flame Ionization D*Wdon Method 3050 Acid digestion Method 3540 Soxhiet sample preparation Mediad 3.150 Sonication sample preparatiou, =traction awthad MediodSQ30 Purgc and trap sample prepinvAon ---Q1A7W --- - - -- uy As CantivT Notes: To avoid false positive detection of benzene, bemene-five solvents are to be used. Fused cap teary coloom are pnf=Tcd to packed ooluinrw, a pa*ed col tram my be used as a"firs cut" with 'dirty" s=ples or once the hits have bees charamdzed mid Mper QA/QC is fbilowvd- For drinking water sources� EPA Tecommends that the 500 series for volatile organic duxdd be used in pmference to the 60 series because the datectim limits are kmm and the QAIQC is better. Samples cd4biting any level of heavy moul contamination may require fielicr analysis. PHS -EM rcoornuvmds holding dine swW1cs until dtspasal is indicated. EM 21046 Ptevised 05/09m) �i F -OXYQEN CLHC TOTAL ATES solo LEAD M 8240 7420 TBA.DIPF- 'ETBF- i 9260 7421 TAMZ Mrs= specifically noted below. Refer to the "SMCB LUFT Field Martual"t Appendix D (B). Table 3-5 on page A7.0 for ininimim, d"et ectim jjpp�,. for Motor V911iCle fuel (gasoline and diesel). Refer to, -Ttj-Re&nal Board Suff Reconarnandations, for bitial Evaluation and kvesogat:Wn of'Ugrs" fbr the waste and motor oil minimut detection limits. Detechon Louts that remain beWw the MCL, STLC or Allowable Limit of the contandnant in question will be aceepted, however laboratory shall utilize the most conservative method. VA-WIRUS) TPH-G Total Petmk-umHydrocarbo�Gasffinc,CC/FD (5030)gOtSnlodorGCWS9260 TpH-D Total Pmoleum HydrombM Diesel, GCTID (3550), 9015 mod or GAS SM 8TX & EBcnzeno, Toluene, Xylene & EtW Be=ene, GOPID 8020 or GCWS 9260 CLK ChWnaWH)*wAftnGCIEWSOI OWMS92400r$260 TOTAL LEAD TOW lead, AA 7420, AA 7421 or 14CP-AES 6010 OXYGENATES UrMEETRE, TAME, D1PF,&TBA GOMS 8260 (For MM=vgL2WXyou =yuse 80M METALS ICAP or AA Inductively Coupled Plasina Atoniic Emission Spedroofty 6010 or Atomic Absorption Spec"itfty 7000 Metals: CatWvn16 Chromium M and V1, Lead, Efte and NWceL PC8 Polyctlorbiated DiphcnyK GOMS 9270 or SM GC -F rD Gas Chromatography, Flame Ionization D*Wdon Method 3050 Acid digestion Method 3540 Soxhiet sample preparation Mediad 3.150 Sonication sample preparatiou, =traction awthad MediodSQ30 Purgc and trap sample prepinvAon ---Q1A7W --- - - -- uy As CantivT Notes: To avoid false positive detection of benzene, bemene-five solvents are to be used. Fused cap teary coloom are pnf=Tcd to packed ooluinrw, a pa*ed col tram my be used as a"firs cut" with 'dirty" s=ples or once the hits have bees charamdzed mid Mper QA/QC is fbilowvd- For drinking water sources� EPA Tecommends that the 500 series for volatile organic duxdd be used in pmference to the 60 series because the datectim limits are kmm and the QAIQC is better. Samples cd4biting any level of heavy moul contamination may require fielicr analysis. PHS -EM rcoornuvmds holding dine swW1cs until dtspasal is indicated. EM 21046 Ptevised 05/09m) �i