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,/16/2005 09:01 20946J"33 EHD <br />10:11,7111i - MIK + ` <br />PAGE 06 <br />TANK TANK TPH-0 TPH-D <br />CONTENTS 8015 8015 <br />13TX & E CL HC TOTAL <br />MTBE AES EN <br />�^� PCB <br />8260 8260 <br />5020 8010 LCAD <br />8260 8240 7420 <br />8020 (nTliiE, <br />8260 TSA,tzrn[, ICRP/ 8270 <br />8260 7421 <br />t 7BL', AES or 8080 <br />TAME) AA <br />8260 <br />L>✓ADED GAS X <br />X <br />x <br />X <br />UNL GAS X <br />X <br />X <br />DI.ESEI, X <br />X <br />KEROSENE X <br />X <br />X <br />UNK FUEL X <br />X <br />X <br />X <br />PROD. OIL <br />X <br />X <br />CHLOR. <br />50LVEN!'S <br />X X <br />X <br />NONCHLOR <br />SOLVENTS }{ <br />X <br />X <br />WASTE\ <br />USED OIL X X <br />X X <br />All analysis methods aro the designated EPA methods described In EPA SW 846, Third Edition. <br />specifically noted below. Refer to the "SWR CB LUFI' Fleld Manual", <br />X X X <br />111 <br />'those methods not found in SW 8a6 are <br />limits for motor vehicic fuel (gasoline and diesel). <br />Investigation <br />Appendix D (B), Table 3-5 on page A20 for minimum detection <br />Refer to "Tri-Rogional Board Staff <br />Rccomm'endations for Initial Evaluation and <br />of US'I"s" for the waste and motor oil minimum detection limits, Detection Limits that remain below tltc MCL, <br />Allowable Limit or the contaminant <br />in question will <br />be accepted, however laboratory shall utilize <br />MC or <br />the most <br />conservative method. <br />LABOR <br />TPH•G Total Petroleum Hydrocarbon, Gasoline, GC/FID)(50 0) 8015 mod orTORY EGC/MS�82600LOGY; <br />TPH•D Total Pcvolcum Hydrocarbon, Diesel, GC/FID (3550), $015 mod or GC/MS 8260 <br />BTX & EBemene, Toluene, Xylcne & Ethyl ,Benzene, GC/PM 8020 or GC/MS 8260 <br />CL HC Chlorioatcd I lydrocarbon, GC/HSD 8010, GC/MS 8240 or $260 <br />TOfA1. LEAD Tota) lead, AA 7420, AA 7421 or [CP -AES 6010 <br />OXYGENATES MTBE, ETBt;, TAME, DiPE, & TBA GC/M5 826 (par MTBE n <br />Cadmium, Chromium Ill and V1, ,Lead, Zine and Nickel. <br />METALS tCAP ur AA Inductively Coupled Plusma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Monis: <br />PCB Polychlorinated Biphenyls, GC/MS 8170 or 8080 <br />CC -FID Gas CJvoma1091`110y, Flame lonination Detection <br />Method 3050 Acid digestion <br />Method 3540 SOxhict sample pmparution <br />Method 3550 Sonication sample preparxion, extraction method <br />Nettled SU30 Purge and trap sample prapuation <br />QA/QC Queli(y Assurunce/Quality Contyo) <br />Notcs: To avoid false positive dctccdon of benzene, ben2cnc-tree solvents arc to be used. Fused capii)aty columns are preferred to packed columns; a <br />packed column may be used ns a "first cut" with "dirty" samples or once the hydrocarbons have been characterized and proper QA/QC is followed. For <br />drinking water Stxirces, EPA recommends that the 500 series for voluble Organic should beused in prrferenec to the 600 Series because the detection <br />limits are lower and the QA/QC is better. Samples cxhib;ting any level of heavy metal contamination may require further analysis. PHS-EHD <br />recorrunend$ holding those samples until disposal is indicated. <br />EH 23 046 (Revised 05/09!00) <br />