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Ames i( an Erl ii o n cental Nc°tot f» k <br /> WORK ORDER 9712342 QUALITY CONTROL REPORT PAGE QR-9 <br /> 1 ANALYSIS Volatile GC/MS <br /> MATRIX Water <br /> METHOD BLANK SAMPLES <br /> SAMPLE TYPE Blank Method/Media blank LAB ID BLNK 1230 INSTR RUN GCM513\971230000000/2/1 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED — BATCH ID MS13W123197 <br /> UNITS ug/L ANALYZED 12/30/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REC LIMITS (%) RPD ' <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT (X) <br /> 1 2 DCA d4 (surr) 102 100 102 65 135 <br /> Toluene d8 (surr) 92 6 100 92 6 70 130 <br /> L p BFB (surr) 104 100 104 70 130 <br /> 1 1 Dichloroethene ND 5 <br /> Benzene NO 5 <br /> Trichloroethene ND 5 <br /> Toluene NO 5 <br /> Chlorobenzene NO 5 <br /> Acetone ND 100 <br /> Bromodichloromethane ND 5 <br /> Bromoform NO 5 <br /> Bromomethane NO 10 <br /> 2-Butanone ND 100 <br /> Carbon Disulfide ND 10 <br /> Carbon Tetrachloride ND 5 <br /> Chloroethane ND 10 <br /> 2 Chloroethyl V,nyl Ether ND <br /> 10 <br /> Chloroform NO 5 <br /> Chloromethane ND 10 <br /> Dibromochloromethane ND 5 <br /> 1 1 Dichloroethane ND 5 <br /> 1 2 Di chloroethane NO 5 <br /> cis 1 2 Dichlaroethene ND 5 <br /> trans 1 2 Dichloroethene ND 5 <br /> 1 2 Oichloropropane ND 5 <br /> cis 1 3 Dichloropropene ND 5 <br /> trans 1,3 D7chloropropene ND 5 <br /> Ethylbenzene ND 5 <br /> 2 Hexanone NO 50 <br /> Methylene Chloride ND 10 <br /> 4 Methyl 2 pentanone ND 50 <br />' Styrene ND 5 <br /> 1 1 2 2 Tetrachloroethane ND 5 <br /> Tetrachloroethene NO 5 <br /> 1 1 1 Trichloroethane ND 5 <br /> 1 1 2 Trichloroethane NO 5 <br /> Vinyl Acetate NO 50 <br /> Vinyl Chloride ND 10 <br /> Xylenes Total ND 10 <br /> 1 2 Dibromoethane ND 5 <br /> 1 2 Dichlorobenzene ND 5 <br /> 1 3 Dichlorobenzene NO 5 <br /> 1 4 Dichlorobenzene NO 5 <br /> Dichlorodifluoromethane ND 10 <br /> Trichlorofluoromethane ND 5 <br />' Tr,chlorotrifluoroethane ND 5 <br /> Tetrahydrofuran ND 50 <br /> Ethanol NO 100 <br /> LABORATORY CONTROL SAMPLES <br /> SAMPLE TYPE Laboratory Control Spike LAB ID LCSW 1230 INSTR RUN GCMS13\971230000000/3/2 <br /> INSTRUMENT HP mass spec for Volatiles PREPARED BATCH ID MS13W123197 <br /> UNITS ug/L ANALYZED 12/30/97 DILUTION 1 00 <br /> METHOD <br /> REF REPORTING SPIKE RECOVERY REG LIMITS (X) RPD <br /> ANALYTE RESULT RESULT LIMIT VALUE (X) LOW HIGH RPD (X) LIMIT {X) <br /> 1 2 DCA d4 (surr) 107 107 100 107 65 135 <br /> Toluene da (surr) 95 2 95 2 100 95 2 70 130 <br /> p BFB (surr) 107 107 100 107 70 130 <br /> 1,1 Dichloroethene 60 3 ND 5 50 0 121 70 130 <br />