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OXY <br /> Glenn SANS Holdings, Inc. <br /> `w'l A subsidiary of Occidental Petroleum <br /> • Nitrate, sulfate and chloride using EPA Method 300.0 <br /> • Organochlorine pesticides (OCPs) using EPA Method 8081 <br /> • Organophosphorous pesticides (OPPs) using EPA Method 8141 <br /> • Herbicides using EPA Method 8151 <br /> Analytical results were reviewed by ARCADIS and summarized below. Copies of the analytical <br /> laboratory reports are included in Attachment 1. The following concentrations were detected in <br /> the liquid characterization samples collected from the UST: <br /> • 28 milligrams per liter(mg/L)TPH-extractable diesel range organics <br /> • 34 mg/L TPH-extractable oil range organics <br /> • 11,000 micrograms per liter(µg/L) sulfolane <br /> • Greater than 600C Flashpoint (non-ignitable) <br /> • Greater than 750 mg/L LC50 (non-toxic) <br /> • Non-detect reactive Cyanide or reactive Sulfide (non-reactive) <br /> • 6.54 pH (non-corrosive) <br /> • 125 mg/L chloride (less than the Secondary Maximum Contaminant Level [MCL] of 250 <br /> mg/L) <br /> • 1.3 mg/L nitrate (less than the Primary MCL of 10 mg/L) <br /> • 34.4 mg/L sulfate (less than the Secondary MCL of 250 mg/L) <br /> TPH-purgeable gasoline range organics, VOCs, DBCP, EDB, OCPs, OPPs and herbicides were <br /> not detected above their analytical laboratory reporting limits in the liquid characterization <br /> samples. <br /> The UST was located within the ongoing source area excavation; therefore on October 11 and <br /> 12, 2011 the liquid was removed from the UST and the UST was moved from the excavation area <br /> and stored on plastic sheeting. This allowed for the continuing of the sulfolane excavation <br /> pending receipt of the liquid characterization sample analytical results. These activities were <br /> completed under the observation of San Joaquin County Environmental Health Department <br /> (SJCEHD) personnel. The liquid was containerized in four 55-gallon steel drums and stored on- <br /> site prior to disposal or treatment using the onsite treatment system. <br /> Sulfolane Information <br /> Sulfolane (tetrahydrothiophene) has been used on site as a cleaning solvent for the pesticide <br /> process equipment. It is readily soluble in water and has a health-based criterion of 57 µg/L in <br /> groundwater approved by the RWQCB. <br /> Closing <br /> Based on the analytical results from the liquid characterization sample collected from the UST, <br /> the liquid does not appear to be hazardous. Therefore, ARCADIS requests a permit exemption by <br /> the SJCEHD pertaining to removal and disposal of the UST and associated UST contents. <br /> 5005 LBJ Freeway, Suite 1350 2 <br /> Dallas,TX 75244-6119 <br />