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Lancaster <br /> 111kiY Laboratories Analysis Report <br /> 25 New Holland Pike PO Box 12425 Lanaasler,PA 17605-2425•717-656 2300 Fax 717-656.2681•www lancasterlabs corn <br /> Page 7 of 8 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 882770 <br /> Reported 02/12/04 at 06 16 PM <br /> Surrogate Quality Control <br /> Blank 109 <br /> LCS 115 <br /> MS 129 <br /> MSD 132 <br /> Limits 57-146 <br /> Analysis Name TPH-GRO - Waters <br /> Batch number 04030AOBB <br /> Trifluorotoluene-F <br /> 4205543 111 <br /> 4205544 110 <br /> Blank 131 <br /> LCS 115 <br /> MS 129 <br /> MSD 132 <br /> Limits 57-146 <br /> Analysis Name TCL SW846 Semivolatiles/Waters <br /> Batch number 04033WACO26 <br /> 2-Fluorophenol Phenol-d6 2,4,6-Tribromophenol Nitrobenzene-d5 <br /> 05541 53 33 63 92 <br /> ank 50 30 87 83 <br /> S 58 35 92 90 <br /> LCSD 55 35 90 89 <br /> Limits 23-94 10-80 45-142 54-124 <br /> 2-Fluorobiphenyl Terphenyl-d14 <br /> 4205541 85 80 <br /> Blank 78 80 <br /> LCS 88 98 <br /> LCSD 88 96 <br /> Limits 64-112 53-124 <br /> Analysis Name EPA SW846/8260 (water) <br /> Batch number N040331AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4205541 95 93 99 98 <br /> Blank 94 95 101 100 <br /> LCS 95 94 99 99 <br /> LCSD 96 93 100 100 <br /> MS 96 92 98 100 <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name STEX+MTBE by 8260B <br /> Batch number P040301AA <br /> Dibromofluoromethane 1,2-❑ichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 4205540 97 97 94 94 <br /> 4205543 96 97 94 93 <br /> 4205544 97 95 95 94 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br />