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Analysis Report <br /> R <br /> Lancaster Laboratories Page 4 of <br /> Whe8eu(H/u liit dY rs a.S�'ence <br /> y Control Summary <br /> Client Name Chevron Products Company Group Number 783870 <br /> Reported 11/30/01 at 05 37 PM <br /> Sample Matrix Quality Control <br /> Ms MSD MS/MSD RPD EKG DUP DUP Dup <br /> RPD <br /> Analysis Name %RSC %REC Limits RPD bmx Conc Conc RPD Max <br /> Methyl tert-Butyl Ether 102 115 60-145 12 30 <br /> TPH-GRO N California (waters) 104 99 74-132 6 20 <br /> Batch number 01304112601A Sample number(s) 3715000 <br /> TRPH 418 1 N D N D 4 (1) 34 <br /> Batch number 013045732001 Sample number(s) 3715001 <br /> Cadmium 102 80-120 N D N D 0 (1) 20 <br /> Chromium 102 80-120 N D 0 0035 200* (1) 20 <br /> Lead 99 80-120 N D N D 0 (1) 20 <br /> Nickel 100 83-115 N D N D 0 (1) 20 <br /> Zinc 100 80-120 0 0115 0 0104 9 (1) 20 <br /> Batch number P013061AC Sample number(s) 3715000 <br /> Chloromethane 71 73 48-132 2 30 <br /> Vinyl Chloride 83 86 54-133 3 30 <br /> Bromomethane 68 67 37-127 1 30 <br /> Chloroethane 81 82 55-129 1 30 <br /> Trichlorofluoromethane 110 111 46-151 1 30 <br /> 1,1-Dichloroethene 108 108 75-152 0 30 <br /> ylene Chloride 100 99 81-134 0 30 <br /> � <br /> 6-1,2-Dichloroethene 102 103 78-140 1 30 <br /> 1-Dichloroethane 105 105 77-142 0 30 <br /> cis-1,2-Dichloroethene 94 96 76--140 1 30 <br /> Chloroform 103 103 76-138 0 30 <br /> 1,1,1-Trichloroethane 108 108 78-141 0 30 <br /> Carbon Tetrachloride 114 114 66-148 0 30 <br /> Trichloroethene 97 97 76-137 0 30 <br /> 1,2-Dichloropropane 84 84 82-128 1 30 <br /> Bromodichloromethane 97 98 81-127 1 30 <br /> 1,1,2-Trichloroethane 92 93 82-127 1 30 <br /> Tetrachloroethene 101 102 72-150 1 30 <br /> Dibromochloromethane 94 95 74-125 1 30 <br /> Chlorobenzene 98 97 81-125 1 30 <br /> Bromoform 84 84 62-127 0 30 <br /> 1,1,2,2-Tetrachloroethane 86 86 70-129 0 30 <br /> 1,3-Dichlorobenzene 97 97 82-128 0 30 <br /> 1,4-Dichlorobenzene 95 94 78-131 1 30 <br /> 1,2-Dichlorobenzene 93 93 82-125 0 30 <br /> trans-1,3-Dichloropropene 85 85 76-124 0 30 <br /> cis-1,3-Dichloropropene 81 81 70-123 0 30 <br /> Freon 113 118 119 70-157 1 30 <br /> Batch number U013041AA Sample number(s) 3715000 <br /> Ethanol 110 123 70-130 11 30 <br /> Methyl t-butyl ether 98 97 69-134 1 30 <br /> di-Isopropyl ether 100 100 75-128 0 30 <br /> Ethyl t-butyl ether 97 96 73-123 1 30 <br /> t-Amyl methyl ether 98 97 69-126 2 30 <br /> t-Butyl alcohol. 96 97 50-157 2 30 <br /> Benzene 102 100 78-134 2 30 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br /> Lancaster Laboratories Inc <br /> M E M 6 E R 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster,PA 17605 2425 <br /> 717-656-2300 Fax 717 656 2681 2216 Rev 9/11/00 <br />