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r <br /> Analysis Report <br /> Lancaster Laboratories Page 6 of 7 <br /> Where��u Irby rs a s Clence <br /> Quity ontrol Summary <br /> Client Name Chevron Products Company Group Number 783870 <br /> Reported 11/30/01 at 05 37 PM <br /> Surrogate Quality Control <br /> LCSD 111 97 <br /> Lamits 65-137 72-134 <br /> Analysis Name TCL SW846 Semivolatilea/Waters <br /> Batch number 01302WACO26 <br /> 2-Fluorophenol Phenol-d6 2,4,6-Tribromophenol Nitrobenzene-d5 <br /> 3715000 26 17 48 98 <br /> Blank 61 41 83 104 <br /> LCS 64 43 88 106 <br /> LCSD 65 43 86 107 <br /> Limits 15-105 10-89 35-147 52-136 <br /> 2-Fluorobiphenyl Terphenyl-d14 <br /> 3715000 90 91 <br /> Blank 93 96 <br /> LCS 98 109 <br /> LCSD 99 113 <br /> Limits 59-117 41-139 <br /> lysis Name SPA SW846/8260 (water) <br /> ch number P413061AC <br /> Dibromofluoromethane 1,2-DYchloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 3715000 107 97 94 90 <br /> Blank 105 96 94 90 <br /> LCS 100 94 96 99 <br /> MS 100 93 97 98 <br /> MSD 100 94 96 99 <br /> Limits 86-118 80-120 88-110 86-115 <br /> Analysis Name SPA SW846/6260 (water) <br /> Batch number U013041AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene <br /> 3715000 94 94 94 91 <br /> Blank 93 97 97 91 <br /> LCS 93 96 96 92 <br /> MS 93 101 94 92 <br /> MSD 95 98 96 93 <br /> Limits 86-116 80-120 88-110 86-115 <br /> Analysis Name MTBE by GC/MS (water) <br /> Batch number U013061AA <br /> Dibromofluoromethane 1,2-DYchloroethane-d4 Toluene-dB 4-Bromofluorobenzene <br /> '3715003 97 99 94 89 <br /> Blank 95 97 93 91 <br /> LCS 96 101 95 91 <br /> *-Outside of specification <br /> The result for one or both determinations was less than five times the LOQ <br /> The background result was more than four times the spike added <br /> Lancaster Laboratories Inc <br /> M E M B E R 2425 New Holland Pike <br /> PO Box 12425 <br /> Lancaster 2 00 17605 2425 <br /> a-nil717-656 2300 Fax 717-656 2691 2216 Rev 9!11!00 <br />