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-- x <br /> _ . <br /> r ¢ 'ICA'�IOI`I IABQ `TORY AN '.I <br /> FNM TSS p�� <br /> trTOTAL EDB 827 <br /> VH-D BTX &E CL HC LEAD ICAPI 80H0 <br /> TANK TANK TPH-G 801,5 8020 8010 8240 AES Or <br /> # CONTENTS 8015 8260 82.40 7420 AA <br /> 8260 82.60 7421 <br /> LEADED X X X X <br /> GAS <br /> UNL GAS X X <br /> DIESEL. �X X <br /> KEROSENE X X <br /> UNK FUEL X X X X X <br /> PROD. OIL X X <br /> i <br /> CHLOR. <br /> SOLVENTS X X <br /> NONCHLOR <br /> SOLVENTS X X X <br /> WASTE\ <br /> USED OIL X X X X X X <br /> All analyses methods are designated EPA methods descn'bed in EPA SW 846, Third Edition. 'Those methods not found <br /> in SW 846, are specifically noted below. Refer to the "SWRCB LUFT Field Manual', Appendix A-20, Table 3-5 for <br /> detection limits of motor vehicle fuels (gasoline and diesel). Refer to 1-2-3 "Regional Board Staff Recommendations for <br /> Initial Evaluation and Investigation of UST's' for the waste and motor oil detection limits. <br /> Detection Limits that remain below the MCL, STLC or Allowable limit of the contaminant in question will be accepted, <br /> however laboratory shall utilize the most conservative method. <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon, Gasoline, GC/FID (5030) 8015 mod or GC/MS 8250 <br /> TPH-D Total Petroleum Hydrocarbon, Diesel, GC/FID (3550), 8015 mod or GC/MS 8260 <br /> BTX & E Benzene,Toluene,Xylene &Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon, GC/HSD 8010, GCJMS 8240 <br /> TOTAL LEAD Total lead, AA 7420, AA 7421 or TCP-AES 6010 <br /> EDB Ethylene dibromide (DHS-AB 1803), GC/MS 8240 (DHS-LUFT) <br /> GC-FID Gas Chromatography, Flame Ionization Detection <br /> ICAP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption <br /> Spectrometry 7000. Metals: Cadmium, Chromium III and VI, bead, Zinc and Nickel.. <br /> PCB Polychlorinated Biphenyls, GC/MS 8270 or W80 <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> Notes: To avoid false positive detection of benzene,benzene-fres solvents are to be used. Fused capillary columns are <br /> preferred to packed columns; a packed column'may be used as a •first cut" with "dirty" samples or once the hydrocarbons <br /> have been characterized and proper QA/AC is followed. <br /> For Drinking water sources, EPA recommends that the 500 series for volatile organics be used in preference to the 600 <br /> series because the detection limits are lower and the QA/QC is better. Samples exhibiting any level of heavy metal <br /> contamination may require further analysis. PHS-EHD recommends holding these samples until disposal is indicated. <br /> EH 23 048 (Revised 7/10192) Page 8 <br /> • iF <br /> S } li <br />