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' Alpha Analytical, Inc. <br /> 255 Glendale Ave • Suite 21 • Sparks,Nevada 89431-5778 <br /> (775)355-1044 -(775)355-0406 FAX • 1-800-283-1183 <br /> ate Work Order <br /> -Jun-03 OC Summary Report 03061709 <br />' Method Blank Type MBLK Test Code EPA Method SW8260B <br /> File ID D 1MSDCHEM1MS121DATA1030619103061905 D Batch ID MS12WO619A Analysis Date 06119!2403 08 58 <br /> Sample ID MBLK MS12WO619A Units pglL Run ID GC/MSD-12-030619A Prep Date 06119!2003 <br />' <br /> Analyte Result PQL SpkVal SpkRefVal %REG LowLimit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene ND 0 5 <br /> Toluene ND 0 5 <br /> Ethylbenzene ND 0 5 <br /> m p-Xylene ND 0 5 <br /> o-Xylene ND 0 5 <br /> Laboratory Control Spike Type LCS Test Code EPA Method SW82608 <br />' File ID DIMSDCHEM1MS121DATA1030619103061904 D Batch ID MS12WO619A Analysis Date 06/1912003 08 37 <br /> Sample ID LCS MS12WO619A Units pg1L Run ID GCIMSD_12_030619A Prep Dale 06119!2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit HighLimit RPD Ref Val %RPD Qual <br />' Benzene 10 3 0 5 10 103 83 119 <br /> Toluene 10 2 0 5 10 102 80 120 <br /> Ethylbenzene 10 0 5 10 100 80 120 <br /> m p-Xylene 19 9 05 20 996 77 124 <br /> o-Xylene 965 0 5 10 97 77 125 <br />' Sample Matrix Spike Type MS Test Code EPA Method SW8260B <br /> File ID D IMSDCHEM1MS121DATA103061910306'1908 D Batch ID MS12WO619A Analysis Date 06!19!2003 10 00 <br />' Sample lD 03061709-01AM50 Units pglL Run ID GCIMSD_12_030619A Prep Date 0611912003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 52 3 1 3 50 0 105 83 119 <br /> Toluene 516 13 50 0 103 80 120 <br /> ylbenzene 544 1 3 50 2 38 104 80 120 <br /> Xylene 103 13 100 0 103 77 124 <br /> o-Xylene 50 2 1 3 50 0 100 77 125 <br />' Sample Matrix Spike Duplicate Type MSD Test Cade EPA Method SW8260B <br /> File ID D 1MSDCHEM1MS121DATA1030619103061909 D Batch ID MS12WO619A Analysis Date 06!1912003 10 20 <br /> Sample ID 03061709-01AMSD Units pglL Run ID GC/MSD-12-030619A Prep Date 06/19/2003 <br /> Analyte Result PQL SpkVal SpkRefVal %REC LowLimit HighLimit RPD Ref Val %RPD Qual <br /> Benzene 51 3 1 3 50 0 103 83 119 52 33 199 <br /> Toluene 50 8 1 3 50 0 102 80 120 51 56 1 5 <br /> Ethylbenzene 53 8 1 3 50 2 38 103 80 120 54 36 1 01 <br /> m p-Xylene 101 1 3 100 0 101 77 124 103 222 <br /> 1 o-Xylene 49 7 1 3 50 0 99 77 125 5018 0 921 <br /> i <br /> Comments ND Not Detected at the Reporting Limit D If the spiked value is X25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery limits M Spike Recovery outside accepted recovery limits due to matrix <br /> S-Analyte detected in the associated Method Blank <br /> 1 <br /> 1 <br /> I <br /> 1 <br /> 1 <br />