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Alpha Analytical, Inc. <br /> 255 Glendale Ave - Suite 21 - Sparks,Nevada 8943 1-5778 <br /> AL (775)355-1044-(775)355-0406 FAX- 1-800-283-1183 <br /> ate QC Summary Report Work Order <br /> -Jan-01 02010962 <br /> ' Method Blank Type MBLK Test Code SW8260B Batch ID MS9S0114A <br /> File ID D1HPCHI=M1MS091DATA1020114102011409 D Analysis Date 01/14/2002 12 53 <br /> Sample ID MBLK MS9S0114A Units pg/Kg Run ID GC/MSD-9-020114A Prep Date 01/1412002 <br /> Anatyte Result PQL SpkVal SpkRefVai %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene ND 5 <br /> Toluene ND 5 <br /> Ethylbenzene ND 5 <br />' m,p-Xylene ND 5 <br /> o-Xylene ND 5 <br /> Laboratory Control Spike Type LCS Test Code SW8260B Batch ID MS9S0114A <br /> File ID D XHPCHEMWS091DATAV020114102011410 D Analysis Date 01/14/2002 13 15 <br /> Sample ID LCS MS9S0114A Units pg/Kg Run ID GCIMSD_9_020114A Prep Date 01/14/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 206 5 200 103 32 148 <br /> Toluene 182 5 200 91 39 136 <br /> Ethylbenzene 191 5 200 95 45 152 <br /> m,p-Xylene 378 5 400 94 42 154 <br /> o-Xylene 198 5 200 99 41 154 <br />' Sample Matrix Spike Type MS Test Code SW8260B Batch ID MS9S0114A <br /> File ID D 1HPCHEMWIS091DATA1020114102011415 D Analysis Date 01/1412002 15 27 <br /> Sample ID 02010962-02AMS Units pg/Kg Run ID GCIMSD_9_020114A Prep Date 01/11/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 156 5 200 0 78 32 148 <br />_Aftuene 139 5 200 0 70 39 136 <br /> (benzene 145 5 200 0 72 45 152 <br /> ,p-Xylene 291 5 400 0 73 42 154 <br /> o-Xylene 151 5 200 0 75 41 154 <br /> Sample Matrix Spike Duplicate Type MSD Test Code SW8260B Batch ID MS9S0114A <br />' File ID D 1HPCHEM%MS091DATA1020114102011416 D Analysis Date 01/1412002 15 50 <br /> Sample ID- 02010962-02AMSD Units pg/Kg Run ID GCIMSD_9_020114A Prep Date 01/11/2002 <br /> Analyte Result PQL SpkVal SpkRefVal %REC Lowl-imit Highl-imit RPD Ref Val %RPD Qual <br /> Benzene 696 5 200 0 35 32 148 156 766 <br /> Toluene 592 5 200 0 30 39 136 1391 806 S <br /> Ethylbenzene 611 5 200 0 31 45 152 1445 81 2 S <br /> m,p-Xylene 126 5 400 0 32 42 154 2909 789 S <br /> o-Xylene 661 5 200 0 33 41 154 1509 781 S <br /> Comments ND-Not Detected at the Reporting Limit D-If the spiked value is<25%of the reference value,recovery should not be calculated <br /> S-Spike Recovery outside accepted recovery(amts M-Spike Recovery outside accepted recovery limits due to matrix <br />' B-Analyte detected in the associated Method Blank <br />