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110 2nd Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http//www mccampbell coin E-mail main@mccampbell com <br /> Advanced GeoEnvtronmental Client Project ID Plaza Liquors 11 <br /> Date Sampled 01/16/02 <br /> 837 Shaw Road Date Received 01/17/02 <br /> Stockton, CA 95215 Client Contact Brian Millman Date Extracted 01/18-01/22/02 <br /> [Client P O Date Analyzed 01/18-01/22/02 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 88359 88360 88361 88362 <br /> MW1/01160 MW2/01160 MW3/01160 MW4/01160 Reporting Limit <br /> Client ID 2 2 2 2 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-tsopropyl Ether(DIPS) ND<500 ND<200 ND<2 5 ND<25 50 10 <br /> Ethyl tent-Butyl Ether(ETRE) ND<500 ND<200 ND<2 5 ND<25 5 0 1 0 <br /> Methyl-tent Butyl Ether(MTBE) 18,000 5200 40 790 5 0 10 <br /> tent-Amyl Methyl Ether(TAME) ND<500 ND<200 ND<2 5 ND<25 50 1 0 <br /> tert-Butanol ND<2500 ND<1000 ND<12 5 ND<125 25 50 <br /> Surrogate Recoveries(%) <br /> Dibromofluoromethane 101 99 110 110 <br /> Comments <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP 1 STLC/SPLP extracts in ug/L <br /> ND means not detected above the reporting limit,N/A means surrogate not applicable to this analysis <br /> (h)lighter than water immiscible sheen is present, (c)liquid sample that contains greater than--5 vol %sediment,0)sample diluted due to <br /> high organic Content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />