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MATRIX SPIKE SAMPLE DATA REPORT <br /> GC/MS Volatiles <br /> Client Lot #. . . : G2E170286 Work Order #. . . : E1WNQIAP-MS Matrix. . . _ _ . . _ . : WATER <br /> MS Lot-Sample #: E2E220298-003 EIWNQ1AQ-MSD <br /> Date Sampled_ . .: 05/22/02 Date Received. . : 05/22/02 <br /> Prep Date. . .. . .: 05/24/02 Analysis Date_ _ : 05/24/02 <br /> Prep Batch #. . . ; 2144227 <br /> Dilution Factor: 1 <br /> r=" SAMPLE SPIKE MEASRD PERCNT <br /> PARAMETER AMOUNT AMT AMOUNT UNITS RECVRY RPD METHOD <br /> Benzene ND 10.0 8.74 ug/L 87 SW846 8260B <br /> ND 10.0 8.51 ug/L 85 2.7 SW846.8260B <br /> 33 Chlorobenzene ND 10.0 9.02 ug/L 90 SW846 82608 <br /> ND 10.0 8.98 ug/L 90 0.44 SW846 8260B <br /> 1,1-Dichloroet~hene ND 10.0 9.16 ug/L 92 SW846 8260B <br /> ND 10.0 9.05 ug/L 90 1_4 SW846 8260B <br /> Toluene ND 10.0 8.91 ug/7a 89 SW846 8260E <br /> ND 10.0 8.82 ug/L 88 1.0 SW046 8260B <br /> ff Trichloroethene ND 10.0 9.83 ug/L 98 SW846 8260B <br /> AID 10.0 9.53 ug/L 95 3.1 SW846 8260B <br /> PERCENT RECOVERY <br /> SURROGATE RECOVERY LIMITS <br /> 3 Bromofluorobenzene 105 <br /> 105 (75 - 130) <br /> 1,2-Dichloroethane-d4 116 (65 - 135) <br /> F=' 112 (65 - 135) <br /> c=� Toluene-d8 100 <br /> ($0 - 130) <br /> 102 (80 - 130) <br /> NOTE(S) : <br /> Calculations are performed before rounding to avoid round-off errors in calculated results. <br /> Bold print denotes control parameters <br /> S=;k <br /> FFFi':V <br /> �`-:='rE170286 STL Sacramento 916-373-5600 40 of 41 <br />