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ASSCA.lAIED LABORATORIES <br /> QA REPORT FORM (MS/MSD) <br />' QC Sample 145838-598825 QC#022505 SO2 <br /> *Matnx SOLID <br /> Prep Date February 25,2005 <br /> Analysis Date February 28,2005 <br /> Lab ID#'s M Batch LR 145838 <br /> REPORTING UNITS= mg/Kg <br />' MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br />' Sample Spike Matnx Matnx %Rec %Rec <br /> TEST JMethod Result ND Added Spike Spike Dup MS MSD RPD <br /> Pb 6010 1- 861 93 84 83 81 80 1 <br /> If Sample Result>4 times Spike Added,then"NC" <br />' ND= "U"-Not Detected <br /> RPD=Relative Percent D�erence of Matrix Spike and Matrix Spike Duplicate %REC LIMITS=75-125 <br /> I0°VoREC-M&EMSD=Percent Recovery of Matnr Spike&Matrix Spike Duplicate JRPD LIMITS —20 <br /> 1 LCSIMB REPORT FORM <br />' LCS Source(s) QC21-LOT#QC2/91/1,QC7-LOT7A92/1 Method BIank <br /> Element Method Result TRUE %Rec L.Lunit H.Limit MB ND <br /> Pb 6010 182 200 91 80% 120% 050 U <br /> Notes RESULT=Sample Result, TRUE=True Value, Yo.Rec=100*Res ult/True <br />' L.LIMIT/HLIMIT=Low/High ControlLimts <br /> MB=Method Blank,ND= "U"for Non-Detected <br />' 3/9/2005 6010 Pb 0225 S2 <br />