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ASSOCIATED LABORATORIES <br /> QA REPORT FORM <br /> QC Sample LR 78153-468 <br /> Matrix WATER <br /> Prep Date 08/19/01 <br /> Analysis Date 08/19/01 -08/20/01 <br /> lD#'s in Batch LR 78425,78426, 78266 78298,78299 <br /> MATRIX SPIKE/MATRIX SPIKE DUPLICATE RESULT <br /> Reporting Units=ug/L <br /> Sample Spike Matrix Matrix %Ree %Ree <br /> Test Method Result Added Spit Spike Du MS MSD RPD <br /> TPH 8015M-G ND 200 232 220 1160 1100 5 3 <br /> Trifluorotoluene Surr 8015M-G 86% 20 223 22 2 1 11 5 1 1 1 0 1 0 4 <br /> ND=Not Detected <br /> RPD=Relative Percent Difference of Matrix Spike and Matrix Spike Duplicate �94REC LIM_!TS 70 -_130_ <br /> ?15RE'C-MS&MSD=Percent Recovery of Matrix Spike&Matrix Spike Duplicate IRPD LIMITS _= 30 _ <br /> PREPARATION BLANK/LAB CONTROL SAMPLE RESULTS <br /> PREP BLK LCS <br /> Test Method Value Result True %Rec L Limit H Limit <br /> TPH 8015M-G ND 234 200 1170 80% 120% <br /> Trifluorotoluene Surr 8015M-G 86% .22_9 20 1145 80% 120% <br /> LCS Result=Lab Control Sample Result <br /> True=True Value of LCS <br /> L Limit/H Limit=LCS Control Limits <br /> 08/31/2001 8015g 0819w1_sur xis <br />