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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425-717-656-2300 Fax:717-656-2681•www.larcasterIabs.com <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgt. Co. Group Number: 1079255 <br /> Reported: 03/12/08 at 01:04 PM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** LOO Units %REC %REC Limits RPD RPD Max <br /> Batch number: 080610017A Sample number(s) : 5289727-5289732 <br /> Total TPH N.D. 4.0 12. mg/kg 95 66-113 <br /> Batch number: 08065SLA026 Sample number(s) : 5289727-5289732 <br /> Naphthalene N.D. 0.00067 0.0017 mg/kg 86 67-105 <br /> Acenaphthylene N.D. 0.00033 0.0017 mg/kg 90 67-100 <br /> Acenaphthene N.D. 0.00067 0.0017 mg/kg 91 73-104 <br /> Fluorene N.D. 0.00067 0.0017 mg/kg 95 75-110 <br /> Phenanthrene N.D. 0.00067 0.0017 mg/kg 97 76-109 <br /> Anthracene N.D. 0.00033 0.0017 mg/kg 92 70-103 <br /> Fluoranthene N.D. 0.00067 0.0017 mg/kg 99 78-114 <br /> Pyrene N.D. 0.00067 0.0017 mg/kg 100 69-116 <br /> Benzo(a)anthracene N.D. 0.00067 0.0017 mg/kg 100 74-112 <br /> Chrysene N.D. 0.00033 0.0017 mg/kg 102 79-111 <br /> Benzo(b)fluoranthene N.D. 0.00067 0.0017 mg/kg 113 70-125 <br /> Benzo(k)fluoranthene N.D. 0.00067 0.0017 mg/kg 109 72-124 <br /> Benzo(a)pyrene N.D. 0.00067 0.0017 mg/kg 99 70-109 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.00067 0.0017 mg/kg 108 64-127 <br /> Dibenz(a,h)anthracene N.D. 0.00067 0.0017 mg/kg 108 46-133 <br /> Benzo(g,h,i)perylene N.D. 0.00067 0.0017 mg/kg 106 58-131 <br /> Batch number: A080601AA Sample number(s) : 5289727-5289732 <br /> Benzene N.D. 0.0005 0.005 mg/kg 112 106 84-115 5 30 <br /> Toluene N.D. 0.001 0.005 mg/kg 112 107 81-116 5 30 <br /> Ethylbenzene N.D. 0.001 0.005 mg/kg 109 102 82-115 6 30 <br /> Xylene (Total) N.D. 0.001 0.005 mg/kg 105 99 82-117 6 30 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 080610017A Sample number(s) : 5289727-5289732 UNSPK: 5289727 <br /> Total TPH 95 91 49-123 4 20 <br /> Batch number: 08065SLA026 Sample number(s) : 5289727-5289732 UNSPK: 5289727 <br /> Naphthalene 88 74 27-145 17 30 <br /> Acenaphthylene 88 76 42-141 15 30 <br /> Acenaphthene 91 76 37-145 17 30 <br /> Fluorene 93 78 51-142 17 30 <br /> Phenanthrene 95 81 18-169 16 30 <br /> Anthracene 96 82 34-161 16 30 <br /> Fluoranthene 100 87 36-165 13 30 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />