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Ln <br />m <br />0_ <br />California Department of Toxic Substances Control <br />W Hazardous Materials Laboratory <br />Q Inorganic Section <br />Quality Assurance Summary for ICP <br />u <br />0 <br />K <br />HML Number: 021049 <br />to 021051 <br />Mo -molybdenum <br />HML Sol] QC Sample <br />Metbad <br />Cid1bration Vedficadan <br />Duplicate Spiked Sampte <br />HML No.: <br />021051 <br />Matrix: <br />SOLID <br />Element <br />0.00 <br />mg/k9 <br />1 500 <br />Blank <br />Standard <br />mg1L <br />23.7 <br />g ike Results <br />P <br />mgJkg <br />Uns iked <br />Spike <br />% Recovery <br />107 <br />found <br />known <br />% <br />m 1L <br />found. <br />known <br />% <br />A. <br />8: <br />RPD <br />esu <br />{mglkgI <br />Added <br />{mg*gi <br />A:' <br />13: <br />As -Arsenic <br />67-4 <br />68.2 <br />98.8 <br /><0.10 <br />10.4 <br />10.0 <br />104 <br />528 <br />528 <br />0.00 <br /><6.Oo <br />500 <br />106 <br />106 <br />®a•Barium' <br />49.6 <br />50.6 <br />98.0 <br /><0.010 <br />10.2 <br />10.0 <br />102 <br />7€.8 <br />76.4 <br />-1.7 <br />106 <br />500 <br />-5.8" <br />-5.9" <br />Be-aIlium <br />3.97 <br />4.11 <br />96.6 <br /><0.005 <br />2.05 <br />2.00 <br />102 <br />104 <br />104 <br />0.00 <br /><0.25 <br />100 <br />104 <br />104 <br />Cd -Cadmium <br />19.2 <br />19.3 <br />99.5 <br /><0.010 <br />10.9 <br />10.0 <br />109 <br />512 <br />513 <br />0.00 <br />2.66 <br />500 <br />.102 <br />102 <br />Co -Cobalt <br />21.8 <br />21.9 <br />99.5 <br /><0.05 <br />10.7 <br />10.0 <br />107 <br />507 <br />50B <br />0.00 <br />7.08 <br />500 <br />100 <br />100 <br />Cr -Chromium <br />25.8 <br />25.7 <br />100 <br />1 <br /><0.08 <br />10.6 <br />10.0 <br />106 <br />1098 <br />i088 <br />2.70 <br />616 <br />500 <br />96.4 <br />94.4 11 <br />CU -CO er"" <br />130 <br />124 <br />105 <br />0.23 <br />9.52 <br />10.0 <br />95.2 <br />101 <br />500 <br />=+; <br />Mo -molybdenum <br />17.5 <br />18.0 <br />97.2 1 <br /><0.10 <br />10.7 <br />10.0 <br />107 <br />1 510 <br />512 <br />0.00 <br /><5.00 <br />1 500 <br />102 <br />102 <br />NI -Wicket" <br />23.7 <br />24.0 <br /><0.05 <br />70.7 <br />10.0 <br />107 <br />5912 <br />5684 <br />3.88 <br />> 5371 <br />600 <br />1182'x* <br />1137 � � <br />Pb -Lead <br />25.8 <br />27.1 <br /><0.10 <br />10.8 <br />10.0 <br />108 <br />3204 <br />3091 <br />24.6 <br />2681 <br />500 <br />105 <br />82.0 <br />Se -Selenium <br />60.6 <br />67.0 <br />]90.44 <br /><0.15 <br />10.4 <br />10.0 <br />104 <br />543 <br />545 <br />0.00 <br /><7.50 <br />500 <br />109 <br />109 <br />TI -Thallium <br />80.6 <br />88.4 <br /><0.20 <br />1G.8 <br />10.0 <br />108 <br />495 <br />501 <br />1.01 <br /><10.0 <br />500 <br />99,0 <br />100 <br />V -Vanadium <br />41.8 <br />38.6 <br /><0-06 <br />9.90 <br />10.0 <br />99.0 <br />484 <br />484 <br />00fl <br /><3.00 <br />500 <br />96.8 <br />96,8 <br />Zn -Zinc <br />139 <br />141 <br /><0.10 <br />10.8 <br />1 70.0 <br />108 <br />2763 <br />2088 <br />15,3 <br />1646 <br />500 <br />103 <br />88.4 <br />Element <br />_ <br />HUL Liquid QC Sample <br />mgJkg <br />found known %gIL-_ <br />Reagent <br />Blank <br />Inorganic Ventures <br />deference Standard <br />nagJL <br />found known <br />% <br />Duplicate Spiked Sample <br />Spike Results m Jk <br />g 9 <br />A: _B: RPD <br />HML No: <br />Uns 'ked <br />Result <br />{mgJkgl <br />Matrix. <br />Spike % Recove <br />Added ry <br />{mgJlcgl - A: B: <br />As -Arsenic <br /><0.10 <br />1.06 <br />1.00 <br />106 <br />Ba-Badurn <br />< 0.010 <br />1.01 <br />1.00 <br />101 <br />se -Beryllium <br /><0.005 <br />0.20 <br />0.20 <br />100 <br />Cd -Cadmium <br />< 0.010 <br />1.07 <br />1.00 <br />107 <br />Co-Cobaft <br /><0-05 <br />1.06 <br />1.00 <br />106 <br />Cr -Chromium <br /><0.08 <br />1.04 <br />1.00 <br />104 <br />Cu -Copper <br /><0.10 <br />1.01 <br />1.00 <br />101 <br />Low recoveries ue to <br />�U P.H.Chern.111 Specialist <br />,-, P.H. Chem I i Zenaida C <br />73 Date Analyzed: 05121/03 <br />s <br />tion o1 Ba es Sulfatel. '" <br />Jarnaff Gercha, Supervisor: <br />Date: <br />