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MINIMUM VERIFICATION LABORATORY ANALYSIS <br /> OXYGEN <br /> TANK TANK TPH-G111260 <br /> TPH-D BTX&E CL HC TOTAL MTBE ATES METAL PCB <br /> 8270 <br /> ## CONTENTS 80158015 8020 8010 LEAD 8020 TBA DIPE, A SPor 8080 <br /> 8260 8260 8240 7420 8260 ETBE, AA <br /> 8260 7421 TAME) <br /> 8260 <br /> X X <br /> LEADED GAS X X <br /> UNI,GAS X <br /> X X <br /> DIESEL X X <br /> X <br /> KEROSENE X X <br /> UNK FUEL X <br /> X X X X <br /> X <br /> PROD.OIL X X <br /> CHLOR. X <br /> SOLVENTS X X <br /> NONCHLOR X <br /> SOLVENTS X X <br /> WASTE\ X X X X <br /> USED OIL X X X <br /> All analysis methods are the designated EPA methods described in EPA SW 846, ird B arable Those metho3-5 on page ds not for minimum found in SW 846 are <br /> on <br /> specifically noted below. Refer to the 'SWRCB LUFT Field Manual App ( ) <br /> limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri-Regional Board Staff Recommendations for Initial Evaluation and <br /> Investigation of UST's" for the waste and motor im'willbe accepted,ton ho�vevtts. Detection er laboratory shallLimits til ze the mosthat remain t conservelow the ative ve meth dC or <br /> Allowable Limit of the contaminant in question <br /> LABORATORY ANALYSES TERMINOLOGY: <br /> TPH-G Total Petroleum Hydrocarbon,Gasoline,GC/FID(5030)8015 mod or GC/MS 8260 <br /> TPH-D Total Petroleum Hydrocarbon,Diesel,GC/FID(3550),8015 mod or GC/MS 8260 <br /> BTX&EBenzene,Toluene,Xylene&Ethyl Benzene,GC/PID 8020 or GC/MS 8260 <br /> CL HC Chlorinated Hydrocarbon,GC/HSD 8010,GC/MS 8240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or ICP-AES 6010 <br /> BA GC/MS 8260(For MTBE screen only you may use 8020) <br /> OXYGENATES MTBE,ETBE,TAME,DIPE,&T <br /> a Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. Metals: <br /> METALS ICRP or AA Inductively Coupled Plasm <br /> Cadmium,Chromium III and VI,Lead,Zinc and Nickel. <br /> PCB Polychlorinated Biphenyls,GC/MS 8270 or 8080 <br /> GC-FID Gas Chromatography,Flame Ionization Detection <br /> Method 3050 Acid digestion <br /> Method 3540 Soxhlet sample preparation <br /> Method 3550 Sonication sample preparation,extraction method <br /> Method 5030 Purge and trap sample preparation <br /> QA/QC Quality Assurance/Quality Control <br /> mns are ed to packed columns;a <br /> d capillary <br /> Notes: To avoid false positive detection"firsof with"dir benzene-freesamples or once the hydroca bons have been characterized land proper QA/QC is followed. For <br /> packed column maybe used as a"first "dirty" be used in <br /> drinking water sources,EPA recommtteds Samthat ples <br /> leshe 5e0xh biting any lev0 series for tel of heavy metalile organic contamination emay require further analysis.PHSt EHDhe tection <br /> limits are lower and the QA/QC is b p <br /> recommends holding those samples until disposal is indicated. <br /> EH 23 046 (Revised 05/09/00) <br /> 5 <br />