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U1 <br />QUALITY CONTROL DATA REPORT <br />Analyte: Beryllium <br />Cadmium <br />Chromium <br />Nickel <br />QC Batch#: ME0925966010MDE <br />ME092596W10MDE <br />ME092596601OMDE <br />ME0925966010MDE <br />Analy. Method: EPA 6010 <br />EPA 6010 <br />EPA 6010 <br />EPA 6010 <br />Prep. Method: EPA 3050 <br />EPA 3050 <br />EPA 3050 <br />EPA 3050 <br />MS/MSD <br />LCS 80-120 80-120 80-120 80-120 <br />Control Limits <br />SEQUFnkai <br />ALYTIC <br />'9 <br />Vyt <br />Project Manager <br />Please Note: <br />The LCS is a control sample of known, interferent -free matrix that is analyzed using the same reagents, <br />preparation, and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br />fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br />the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br />interference, the LCS recovery is to be used to validate the batch. <br />'* MS= Matrix Spike, MSD= MS Duplicate, RPD= Relative % Difference 9609D08.SSS < 1 > <br />Analyst: <br />C. Medefesser <br />C. Medefesser <br />C. Medefesser <br />C. Medefesser <br />MS/MSD #: <br />9609D7001 <br />96ND7001 <br />96MD7001 <br />96MD7001 <br />Sample Conc.: <br />0.64 <br />0.68 <br />38 <br />53 <br />Prepared Date: <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />Analyzed Date: <br />Instrument I.D.#: <br />9/25/96 <br />MTJA2 <br />9/25/96 <br />MTJA2 <br />9/25/96 <br />MTJA2 <br />9/25/96 <br />MTJA2 <br />Conc. Spiked: <br />100 mg/Kg <br />100 mg/Kg <br />100 mg/Kg <br />100 mg/Kg <br />Result: <br />100 <br />98 <br />130 <br />150 <br />MS % Recovery: <br />99 <br />97 <br />92 <br />97 <br />Dup. Result: <br />MSD % Recov.: <br />100 <br />99 <br />98 <br />97 <br />140 <br />102 <br />150 <br />97 <br />T <br />RPD: <br />0.0 <br />0.0 <br />7.4 <br />0.0 <br />L_................. <br />RPD Limit: <br />0-20 <br />0-20 <br />0-20 <br />. <br />0-20 <br />MS/MSD <br />LCS 80-120 80-120 80-120 80-120 <br />Control Limits <br />SEQUFnkai <br />ALYTIC <br />'9 <br />Vyt <br />Project Manager <br />Please Note: <br />The LCS is a control sample of known, interferent -free matrix that is analyzed using the same reagents, <br />preparation, and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br />fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br />the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br />interference, the LCS recovery is to be used to validate the batch. <br />'* MS= Matrix Spike, MSD= MS Duplicate, RPD= Relative % Difference 9609D08.SSS < 1 > <br />LCS #: <br />BLK092596 <br />BLKM2596 <br />BLK092596 <br />BLK092596 <br />Prepared Date: <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />Analyzed Date: <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />9/25/96 <br />Instrument I.D.#: <br />MTJA2 <br />MTJA2 <br />MTJA2 <br />MTJA2 <br />Conc. Spiked: <br />100 mg/Kg <br />100 mg/Kg <br />100 mg/Kg <br />100 mg/Kg <br />LCS Result: <br />110 <br />100 <br />110 <br />110 <br />LCS' Recov.: <br />110 <br />100 <br />110 <br />110 <br />MS/MSD <br />LCS 80-120 80-120 80-120 80-120 <br />Control Limits <br />SEQUFnkai <br />ALYTIC <br />'9 <br />Vyt <br />Project Manager <br />Please Note: <br />The LCS is a control sample of known, interferent -free matrix that is analyzed using the same reagents, <br />preparation, and analytical methods employed for the samples. The matrix spike is an aliquot of sample <br />fortified with known quantities of specific compounds and subjected to the entire analytical procedure. If <br />the recovery of analytes from the matrix spike does not fall within specified control limits due to matrix <br />interference, the LCS recovery is to be used to validate the batch. <br />'* MS= Matrix Spike, MSD= MS Duplicate, RPD= Relative % Difference 9609D08.SSS < 1 > <br />