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r. = <br />0 • <br />XIINI,titUtil VERIFICATION LABORATORY ANALYSIS <br />TANK <br />TANK <br />i <br />TPH-G <br />TPH-D <br />BTX & E <br />CL HC <br />TOTAL <br />MTBE <br />mxvrs.�nc <br />twt.. <br />`'FT^a-N <br />PCB <br />CONTENTS <br />8015 <br />8015 <br />8020 <br />3010 <br />LEAD <br />80_0TWA-MPF. <br />[CAP" <br />8_70 <br />4260 <br />8260 <br />8260 <br />8240 <br />7420 <br />8260 <br />AF's <br />TAMS:) <br />or <br />8080 <br />8260 <br />7421 <br />8260 " <br />4A <br />LEADED CrA <br />X <br />X <br />X <br />X <br />UNL GAS I <br />X <br />X <br />X <br />DIESEL <br />X <br />X <br />X <br />KEROSENE <br />X <br />X <br />X <br />UNK FUEL <br />X <br />X <br />X <br />X <br />X <br />PROD. OIL I <br />X <br />X <br />X <br />I <br />CHLOR. <br />SOLVENTS <br />X <br />X <br />X <br />I <br />NONCHLOR <br />SOLVENTS <br />X <br />X <br />X <br />WASTE% <br />USED OIL <br />X <br />X <br />XX <br />X <br />X <br />) <br />All analysis methods are the <br />desienaced EPA <br />mencais deccriberi i., PPA cW QA4 rt,;.A t:,t;.:.... ,�.,, _ _a.c..A_ __. ___� •_ <br />-.:- -- - -- - -------------•-___ �. -... .+w. ' u'Au �.0 "j". t uwa U emous lot touna to <br />SW 846 are specifically noted below. Refer to the "SWRCB LUFT Field Manual", Appendix D (B), Table 3-5 on page A20 for <br />minimum detection limits for motor vehicle fuel (gasoline and diesel). Refer to "Tri -Regional Board Staff Recommendations for <br />Initial Evaluation and Investigation of UST's" for the waste and motor oil minimum detection litnits. <br />Detection Limits that remain below the NICL, STLC or Allowable Limit of the contaminant in question will be accepted, <br />however laboratory shall utilize the most conservative method. <br />LABORATORY ANALYSES TER�IIINOLOGY: <br />TPFI-G Total Petroleum Hydrocarbon. Gasoline. GC/FID (5030) 8015 mod or GC/NIS 8260 <br />TPH-D Total Ptarolcutn Hydrocarbon. Diescl. GC/FID (3550). 8015 mod or GC/MS 8260 <br />BTX & E Benzene. Toluene. Xylene & Ethyl Benzene, GC/PID 8020 or GC/MS 8260 <br />CL HC Chlorinated Hydrocarbon. GC/HSD 8010. GC/MS 8240 or 8260 <br />TOTAL LEAD Total lead, AA 7420. AA 7421 or ICP -AES 6010 <br />OXYGENATES M'rBE. ETBE. TAME. DIPE, & TBA GC/MS 8260 (For MTBE screen only you may use 8020) <br />META! -5 ICRP or AA Inductively Coupled Plasma Atomic Emission Spectrometry 6010 or Atomic Absorption Spectrometry 7000. <br />Metals: Cadmium. Chromium III and VI, Lead. Zinc acid Nickel. <br />PCB Polychlorinated Biphenyls, GC/MS 8270 or 8080 <br />GC -FID Gas Chromatography, Flame Ionization Detection <br />Method 3050 Acid digestion <br />Methtxl 3540 Soxhlct sample preparation <br />Method 3550 Sonication sample preparation, extraction method <br />Method 5030 Purge ;and crap sample preparation <br />QA/QC Quality Assurance/Quality Control <br />Notes: To avoid False positive detection of benzene, hcrtzene-free solvents art: to be used. Fused capillary columns arc prcfcrred to packed <br />columns: a packed column may be used as a "first cut" with 'dirty' samples or once the hydrocarbons have been characterized and proper <br />QA/QC is followed. <br />For drinking water sources. EPA recommends that the 500 series for volatile organic should be used in preference to the 600 series because the <br />detection limits are tower and the QA/QC is better. Samples exhibiting any level of heavy metal contamination may require further analysis. <br />PHS-EHD recommends holding those samples until disposal is indicated. <br />EH 23 046 (Revised 08/13/99) Page 3 <br />