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OCT-07-2003 TUE 11:00 AM GETTLER RYAN FAX NO, 7077893218 P. 07 <br /> V-U-1W;ek5V;e IV,09 20946AdL3 FIFTH FLOOR PAGE 06 <br /> MlN1MUAA VERIFICATION LA130RATORY ANALYSIS <br /> d-TAL <br /> y <br /> ]CAP/ <br /> AES <br /> or <br /> OXYGEN <br /> TANK TANK TPH-G TP14-E) BTX CL HC TOTAL ATE:S MITAL PCM <br /> CONTENTS 8015 8015 8020 8010 LF-AD 0=2 0 (MTBti. <br /> 5. <br /> 8260 8260 8260 9240 7420 8260 TBA10RE, ]GAP/ 82700 <br /> 9260 7421 ME. AES of 80800 <br /> TAMS) <br /> AA <br /> LEADED GAS x x x <br /> UNL GAS x <br /> X <br /> I", SEL x x <br /> KEROSENE x x <br /> NK FUEL x x <br /> +UV x x <br /> ?ROD.OIL x x x <br /> ClMok <br /> SOLVENTS x x x <br /> WONCHLOR <br /> SOV-BENTS x x x <br /> WASTE\ <br /> USED OIL x X x x <br /> x x x <br /> All analysis me&*&are The cic`�- <br /> SlgMtr-d BPA methods described in lYA SW 846,Third Edition Those Meftds not found in 9W 846 axe <br /> specifically noted below. Refer to tble IISWRCB LUFT Field Manualv.AppebdixD(P),Table 3-5 OUPW A-20 for Minimum detcerrion <br /> l"n"sfor me'tar "hir,1C fillel (SasohDe and diesel). Refer to -7r1.RgionalBoard Staff ROCOn=ndStions for Initial Evaluation eared <br /> ltvest'gatiOz Of USTs"far the',Mte and motor oil minim=detection limits_ Detection Limits that remain below the MCL.STLC-'or <br /> Allowable LIFWt of the WAtaminaut in question will be accepted,however laboratory shall utiji2a,the.Most couserv;ative method. <br /> Y-ABOIRATORY ANALYSES TERMINOLOGY: <br /> Tgtal?e=leumH�*CCaTbon-03SOline,GC/FID(5030)90]5trod otWmsa260 <br /> TPH-1) Total PeTrOJOUMHyftcarborl,Diesel,GC/FID(1550),sols mod orryms 8260 <br /> 1377(&E Benzene,Toluene,Xylene&Ethyl ac=cng,GC/pID 8020 07 GC/MS 4260 <br /> CL HC Chlorinated Hydrocarbon,(3C1HSD 601 0,OCIMS 9240 or 8260 <br /> TOTAL LEAD Total lead,AA 7420, AA 7421 or JCP-AES 6010 <br /> Oxyr'&ATES MTtIE,ETRE,TAME,DIPS,&TBA GCNS8260(Por Mf3EjUUnonj you may use 8020) <br /> METAL$ICAP or AA Inductively Coupled plasma Atomlc Emission SpectrDmevy 6010"Atomic Absorption Spectrometry WOO, Met2js,.,. <br /> CA(lad ,Chromimin V1 <br /> PCB PolYchlorinawd 81,phonyls,urnGCA4S$270 orIII$080and 'Lead,Zitic and Nickel <br /> GC'FID Gm Chrommography,Flame jonizallon Dc;teerjon <br /> Method 3050 Arad digestion <br /> Mrthod 3540 Soxh)ct sample preparation <br /> Method 3:550 Sonication sample preparation.extraction=hod <br /> Method$030 Purge acrd trap sample preparation <br /> QA/QC Quality AssurancelQuahty Control <br /> Notes: To avoid false Positive dcWtion of benzene,bemcnc-free solvents are to be Used. Posed capillary columns are prefervd to Packed columns-a <br /> packed column may be used as a"first cut"with"dirty"samples Or once the hydrocarbons have beem characterized and proper QA/QC isfpllowed,columns; <br /> drinking water souses,EPA rftornmonds that the 500 Series for volatile Organic should be used in prafrrcnce to the 600 series because the detection <br /> limits am lower arid the QA)QQ is better, Sampim cz6f"biting any level of heavy mesal contarnirAtion rosy require rJThcr iI ys,s.P S_E D <br /> recommends holding those samples until disposal is indicated. <br /> anal H <br /> EH 25 046 (Revised 05/09/00) Page 5 <br /> JAN 25 ' 02 9: 12 2121946 3433 PAGE.01E35 <br />