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Pace Analytical services,Inc. <br /> aceAnalytical a 2795 Second Street-Suite 300 <br /> Davis,CA 95618 <br /> watvpecelabs.com <br /> (530)297-4800 <br /> • QUALITY CONTROL DATA <br /> Project: Parcel 2A(206397/211321 &P66 <br /> Pace Project No.: 1259724 <br /> OC Batch: DAVM/2917 Analysis Method: EPA 82608 <br /> QC Batch Method: EPA 8260B Analysis Description: 8260 MSV UST Water <br /> Associated Lab Samples: 1259724006, 1259724007,1259724008,1259724009,1259724010, 1259724011, 1259724012, 1259724034, <br /> 1259724035, 1259724036,1259724037 <br /> METHOD BLANK: 281885 Matrix: Water <br /> Associated Lab Samples: 1259724006, 1259724007,1259724008, 1259724009, 1259724010,1259724011,1259724012,1259724034, <br /> 1259724035, 1259724036,1259724037 <br /> Blank Reporting <br /> Parameter Units Result Limit Analyzed Qualifiers <br /> Benzene ug/L ND 0.50 01/15/16 10:30 <br /> Ethylbenzene ug/L ND 0.50 01/15/16 10:30 <br /> Methyl-tert-butyl ether ug/L NO 0.50 01/15/1610:30 <br /> tert-Butyl Alcohol ug/L NO 5.0 01/15/1610:30 <br /> Toluene ug/L NO 0.50 01/15/16 10:30 <br /> TPH as Gas ug/L NO 50.0 01/15/16 10:30 <br /> Xylene(Total) ug/L NO 1.0 01/15/1610:30 <br /> 1,2-Dichloroethane-d4(S) %. 109 70-130 01/15/16 10:30 <br /> 4-Bromofluorobenzene(S) %. 94 70-130 01/15/1610:30 <br /> Toluene-d8(S) %. 101 70-130 01/15/1610:30 <br /> •LABORATORY CONTROL SAMPLE: 261888 <br /> Spike LCS LCS %Rec <br /> Parameter Units Conic. Result %Rec Limits Qualifiers <br /> Benzene ug/L 40 41 102 75-125 <br /> Ethylbenzene ug/L 40 44 111 75-125 <br /> Methyl-tert-butyl ether ug/L 40 39 97 73-125 <br /> tert-Butyl Alcohol ug/L 400 450 113 75-125 <br /> Toluene ug/L 40 42 106 75-125 <br /> Xylene(Total) ug/L 120 120 103 75-125 <br /> 1,2-Dichloroethane-d4(S) %. 101 70-130 <br /> 4-Bromofluorobenzene(S) %. 98 70-130 <br /> Toluene-d8(S) %. 101 70-130 <br /> MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 281887 281888 <br /> MS MSD <br /> 1259724034 Spike Spike MS MSD MS MSD %Rec Max <br /> Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual <br /> Benzene ug/L ND 40 40 38 39 95 97 75-125 2 30 <br /> Ethylbenzene ug/L ND 40 40 42 42 104 105 74-125 1 30 <br /> Methyl-tert-butyl ether ug/L 14 40 40 52 53 96 97 73-129 1 30 <br /> ten-Butyl Alcohol ug/L 18 400 400 430 420 102 101 65.128 1 30 <br /> Toluene ug/L ND 40 40 40 41 100 102 75-125 2 30 <br /> Xylene(Total) ug/L NO 120 120 120 120 96 98 61-129 1 30 <br /> 1,2-Dichloroethane-d4(S) %. 107 106 70-130 <br /> 4-Bromofluorobenzene(S) %. 100 98 70-130 <br /> Toluene-d8(S) %. 103 103 70-130 <br /> Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the dight of the result. <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full. <br /> Date:01/28/2016 07:00 PM without the written consent of Pace Analytical Services.Inc.. Page 37 of 49 <br />