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Pace Analytical Services,Inc. <br /> 2795 Second Street-Suite 300 <br /> aceAnalytical Davis,2995618 <br /> w ..pacelebs.co. (530)297-0800 <br /> • ANALYTICAL RESULTS <br /> Project: Parcel 2A <br /> Pace Project No.: 1259806 <br /> Sample: MID-4 Lab ID: 1259806005 Collected: 01/14/16 10:15 Received: 01/14/16 12:50 Matrix: Water <br /> Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual <br /> 8015 GCS Water Analytical Method:EPA 80158 Preparation Method:EPA 3511 <br /> TPH-DRO(C10-C28) NO mg/L 0.050 1 01/15/16 11:28 01/21/1617:19 <br /> TPH-Motor Oil ND mg/L 0.10 1 ot/15/1611:28 01/21/1617:19 64742-65-0 <br /> Surrogates <br /> n-Octacosane(S) 110 %. 75-150 1 01/15/16 11:28 01/21/1617:19 630-02-4 <br /> 8260 MSV UST Water Analytical Method:EPA 82608 <br /> tert-Amylmethyl ether ND ug/L 0.50 1 01/16/16 01:03 994-05-8 <br /> Benzene NO ug/L 0.50 1 01/16/16 01:03 71-43-2 <br /> tert-Butyl Alcohol NO ug/L 5.0 1 01/16/16 01:03 75-65-0 <br /> Diisopropyl ether NO ug/L 0.50 1 01/16/16 01:03 108-20-3 <br /> Ethylbenzene NO ug/L 0.50 1 01/16/16 01:03 100-41-4 <br /> Ethyl-tert-butyl ether ND ug/L 0.50 1 01/16/16 01:03 637-92-3 <br /> Methyl-tert-butyl ether NO ug/L 0.50 1 01/16/16 01:03 1634-04-4 <br /> Toluene NO ug/L 0.50 1 01/16/16 01:03 108-88-3 <br /> TPH as Gas NO ug/L 50.0 1 01/16/16 01:03 <br /> Xylene(Total) NO ug/L 1.0 1 01/16/16 01:03 1330-20-7 <br /> Surrogates <br /> 1,2-Dichloroethane-d4(S) 110 %. 70-130 1 01/16/16 01:03 17060-07-0 <br /> AMbluene-d8(S) 100 %. 70-130 1 01/16/16 01:03 2037-26.5 <br /> 4-Bromofluorobenzene(8) 98 %. 70-130 1 01/16/16 01:03 460-00-4 <br /> Sample: GW-EFF Lab ID: 1259806006 Collected: 01/14/16 10:00 Received: 01/14/16 12:50 Matrix: Water <br /> Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual <br /> 8015 GCS Water Analytical Method:EPA 8015B Preparation Method:EPA 3511 <br /> TPH-DRO(C10-C28) 0.060 mg/L 0.049 1 01/15/1611:28 01121/16 17:54 DE <br /> TPH-Motor Oil ND mg/L 0.099 1 01/15/16 11:28 01/21/16 17:54 64742-65-0 <br /> Surrogates <br /> n-Octacosane(S) 110 %. 75-150 1 01/15/16 11:28 01/21/16 17:54 630-02-4 <br /> 8260 MSV UST Water Analytical Method:EPA 82608 <br /> tert-Amylmethyl ether NO ug/L 0.50 1 01/16/1601:28 99405-8 <br /> Diisopropyl ether NO ug/L 0.50 1 01/16/16 01:28 108-20-3 <br /> Ethyl-tert-butyl ether NO ug/L 0.50 1 01/16/16 01:28 637-92-3 <br /> TPH as Gas NO ug/L 50.0 1 01/16/16 01:28 <br /> Surrogates <br /> 1,2-Dichloroethane-d4(S) 110 %. 70-130 1 01116/16 01:28 17060.07-0 <br /> Toluene-d8(S) 101 %. 70.130 1 01/16/16 01:28 2037.26-5 <br /> 4-Bromofluorobenzene(S) 96 %. 70.130 1 01/16/16 01:28 460-00-4 <br /> 1664 HEM,Oil and Grease Analytical Method:EPA 1664 OG <br /> Oil and Grease NO mg/L 5.1 1 01/20/16 12:42 <br /> REPORT OF LABORATORY ANALYSIS <br /> This report shall not be reproduced,except in full, <br /> Date:02/03/2016 11:37 AM without the written consent of Pace Analytical Services,Inc.. Page 7 of 27 <br />