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PRECISION (-) <br /> ESO-TE&H <br /> Analytical Laboratory CERTIFICATE OFANALYSIS <br /> Tuesday, March 13, 2007 <br /> Attention: G uy W.Roy <br /> R&L Diesel Report Page 4 of 23 <br /> P.O.Box 2498 <br /> Danville, CA 94526 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sample Informt,tion <br /> Sample ID: Over Tank Sample Type: Grab <br /> Laboratory ID: 7022608-01 Project Name: UST-Waste Oil <br /> Date/Time Sampled: 26-Feb-07 00:00 by Guy W.Roy Sample Matrix: Soil <br /> Test Parameter Result DLR Unit Dilution Batch Peepared Analysis Date Method Notes <br /> 1,2-Dichloroethane ND 2.00 uglkg 1 A372708 27-Feb-07 27-Feb-07 EPA 82606 j <br /> 11-Dichloroethene NO 2.00 uglkg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> cis-1,2-Dich loroethene NO 2.00 ug/kg 1 872708 27-Feb-07 27-Feb-07 EPA 82606 <br /> trans-1,2-Dichloroethene NO 2.00 ug/kg 1 872708 27-Feb-07 27-Feb-07 EPA 6260B <br /> 1,2-Dichloropropane NO 2.00 ug/kg 1 B72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,3-Dichloropropane NO 2.00 uglkg 1 B72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 2,2-Dichloropropane NO 2.00 ug/kg 1 B72708 27-Feb-07 27-Feb-07 EPA 82606 <br /> 1,1-Dichloropropene NO 2.00 ug/kg 1 B72708 27-Feb-07 27-Feb-07 EPA 82608 <br /> cis-1,3-Dichloropropene ND 2.00 ug/kg 1 872708 27-Feb-07 27-Feb-07 EPA 8260B <br /> trans-1,3-Dichloropropene NO 2,00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Ethylbenzene NO 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 82606 <br /> Freon 113 ND 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Hexachlorobutadiene NO 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 2-Hexanone NO 50.0 ug/kg 1 4B72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Isopropylbenzene NO 2.00 ug/kg 1 AB72708 27-Feb47 27-Feb-07 EPA 82608 <br /> p-Isopropyltoluene NO 2.00. uglkg 1 1372708 27-Feb-07 27-Feb-07 EPA 82606 <br /> Methylene chloride NO 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 4-Methyl-2-pentanone NO 20.0 ug/kg 1 872708 27-Feb-07 27-Feb-07 EPA 82606 <br /> Naphthalene NO 2.00 ug/kg 1 A872708 27-Feb-07 27-Feb-07 EPA 8260B <br /> n-Propylbenzene NO 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 82606 <br /> Styrene NO 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,1,2,2-Tetrachloroethane NO 2.00 ug/kg 1 AB727G8 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,1,1,2-Tetrachloroethane NO 2.00 uglkg 1 AB72708 27-Feb-07 27-Feb-07 EPA 82608 <br /> Tetrachloroethene NO 2.00 ug/kg 1 B72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Toluene NO 2.00 ug/kg 1 B72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,2,3-Trichlorobenzene NO 2.00 ug/kg 1 1372708 27-Feb-07 27-Feb-07 EPA 82608 <br /> 1,2,4-Trichlorobenzene ND 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 82606 <br /> 1,1,2-Trichloroethane NO 2.00 uglkg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,1,1-Trichloroethane NO 2.00 ug/kg 1 872708 27-Feb-07 27-Feb-07 EPA 8260B <br /> mg/L=milligrams per Liter-ppm DLR-Detection Limit for Purpose ofReponing. <br /> u9T=micrograms per Liter=ppb Exceptional sample matrices or interferences may <br /> result in higher detection limits. <br /> RESPECTFULLY SUBMITTED, <br /> ��/Otr� <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave Stockton CA. 95204 Dhone: (209) 4 r <br /> 8105 Fax: (209) 477-8148 <br />