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PRECISION'r) n <br /> 4_ <br /> EIMRO-TECH <br /> Analytical Laboratory CERTIFICATE OFANALYSIS_ <br /> Tuesday,March 13, 2007 <br /> Attention: Guy W.Roy <br /> R&L Diesel Report Page 12 of 23 <br /> P.O.Box 2498 , <br /> Danville, CA 94526 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> _ Sample Inform ian <br /> Sample ID: Under Tank Sample Type: Grab <br /> Laboratory ID: 7022608-02 Project Name: UST-Waste Oil <br /> Date/Time Sampled: 26-Feb-07 00:00 by Guy W.Roy Sample 1lfatrbr. Soil <br /> .Test Parameter Result DLR Unit Dilution Batch Prepared Analysis Date Method Notes <br /> Trichloroethene ND 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 82608 I <br /> Trichlorofluoromethane _ ND 2.00 ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,2,3-Trichloropropane ND 2.00 . ug/kg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> 1,3,5-Trimethylbenzene 28.2 2.00 uglkg 1 AB72708 27-Feb-07 27-Feb-07 EPA 8260E <br /> 1,2,4-Trimethylbenzene 95.5 2.00 ug/kgAIA <br /> 72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Vinyl acetate ND 20.0 ug/kg72708 27-Feb-07 27-Feb-07 EPA 82608 <br /> Vinyl chloride ND 2.00 ug/kg72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> Methyl tert-butyl Ether(MtBE) ND 2.00 uglkg72708 27-Feb-07 27-Feb-07 EPA 8260E <br /> Ethyl tert-Butyl Ether(ETBE) ND 2.00 ug/kg72708 27-Feb-07 27-Feb-07 EPA 8260B <br /> m,p-Xylene 23.2 2.00 uglkg 1 A 372708 27-Feb-07 27-Feb-07 EPA 8260E <br /> tert-Amyl Methyl Ether(TAME) ND 2.00 ug/kg 1 A 372708 27-Feb-07 27-Feb-07 EPA 82606 ! <br /> o-Xylene 27.6 2.00 ug/kg 1 A372708 27-Feb-07 27-Feb-07 EPA 82608 <br /> tert-Butyl Acohol(TBA) ND 50.0 uglkg 1 A 372708 27-Feb-07 27-Feb-07 EPA 82608 <br /> Diisopropy!Ether(DIPE) ND 2.00 ug/kg 1 A1372708 27-Feb-07 27-Feb-07 EPA 82608 <br /> Surrogate:Dibromofluoromethane 114% 86-118 <br /> Surrogate:Toluene-d8 110% 88-110 <br /> Surrogate:4-Bromofluorobenzene 108% 86-115 <br /> mg/L=milligrams per Liter=ppm DLR—Detection Limit for Purpose ofReporting. <br /> ug/L=micrograms per Liter=pph Exceptional sample matrices or interferences may <br /> result in higher detection,limits. <br /> RESPECTFULLY SUBMITTED, <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave Stockton CA. 95204 phone: (209) 47 -8105 Fax: (209) 477-8148 k <br /> I <br />