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y <br /> PRECISION <br /> I <br /> ENVIRO-TECH <br /> Analytical Laboratory CERTIFICATE OFANALYSIS <br /> Friday,June 20,200$ <br /> Attention: Guy W.Roy <br /> R&L Diesel Report Page 31 affil <br /> P.O.Box 2498 <br /> Danville,CA 94526 <br /> Volatile Organic Compounds by EPA Method 82606 <br /> Sample informario,n ' <br /> Sample ID: B4 -29 Sample Type: Grab <br /> Laboratory ID: 8030609-07 Project Name: UST-Waste Oil <br /> DatelTime Sampled.• 06-Mar-08 14:15 by Guy W.Roy Sample Matrix: Soil I <br /> I <br /> Test Parameter Result DLR Unit Dilution #afch Prepared Analysis Dale Method Notes <br /> Acetone NO 100 ug/kg 1 A 81102 11-Mar-08 11-Mar-08 EPA 82606 <br /> Benzene NO 2.00 ug/kg i A 81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Bramobenzene — ND 2.00 uglkg 1 A 81102 11-Mar-08 11-Mar-0B EPA 82608 — <br /> Bromochloromethane NO 2.00 uglkg 1 A 1102 11-Mar-08 11-Mar-08 EPA 82606 - <br /> Bromodichloromethane NO 2,00 ug/kg —1 A 81102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Brornoform NO 2.00 ug/kg 1 A 81102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Bromornethane — — — �NO 2,00 ug/kg 1 - A 1102 11-Mar-08 11-Mar-08 EPA 8260E <br /> 2-Butanone NO- —20.0 uglkg� 1 A 1102 11-Mar-08 11-Mar-08 EPA 82608 -—� <br /> n-Butylbenzene NO 2.00 uglkg 1 A 1102 11-Mar-08 11-Mar-08 EPA 8260B <br /> see-Butylbenzene — -- — NO -- 2.00 ugtkg 1 AC 1102 11-Mar-08 11-Mar-0B EPA 82609 <br /> tert-Butylbenzene NO 2.00 uglkg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Carbon disulfide NO 20.0 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Carbon tetrachloride NO 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82606 <br /> Chlorobenzene NO 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82606 <br /> Chlarosthan, NO 2.00 uglkg i AC 1102 11-Mar-0B 11-Mar-08 EPA 8260B <br /> 2-6hloroe7hylvinyl ether — NO 20.0 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82606 <br /> Chloroform — - -- NO 2.00 ug/kg 1... AC 1102 _ 11-Mer-08 11-Mar-08 EPA 6260B <br /> Chloromethane NO — 2.00 ug/kg 1 AC 1102 11-Mar-08 —11-Mar-08 EPA 8260B <br /> .— _ <br /> 2-Chlorototuene NO 2.00 � — 11-Mar-08 <br /> --- — — <br /> glkg 1 AC 1102 i 1-Mar-08 11-Mar-08 EPA 82606 ! <br /> 4-Chlorototuene NO 2.00 uglkg 1 —AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Dib romochloromethane ND 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar 08 EPA 82608 <br /> — —.. <br /> 12-Dibromo-3-chloropropane NO 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 1,2-0ibromoethane(EDB) NO 2.00 ug/kg 1 -AC 1102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Dibromomethane NO 2.00 uglkg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 1,2-Dichlorobenzene NO 2,00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 8260B <br /> 1,3•Dichlorobenzene NO — 2.00 ugrkg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82609 <br /> 1,4-Dichlorobenzene NO 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82646 - <br /> Dichioroddluoromethane ND 2.00 ug/kg 1 AC 1102 11-Mar-W 11-Mar-D8 EPA 8260B <br /> 1,1-Dichloroethane ND 2.00 ug/kg 1 AC 1102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 'Pig L-mirligrwms per Liter„mm DLR-Demc'lon f imir forPurp a ofRepuning. <br /> nrecrogranrs per firer-ppb Fsceprional sampre matrices or rnrerlerern:s may <br /> result in higherdereenon limits. <br /> RESPECTFULLY SUBMITTED, <br /> ��—J/Ot�w �r <br /> Jonathan Le,Laboratory Director <br /> 3935 1% Coronado Ave Stockton CA, 95204 Phone: (209) 477--5105 Fax: f209)5414-7497 <br />