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r <br /> k <br /> CERTIFICATE OF ANALYSIS Analyticaf Laboratory <br /> Friday,April 4, 2008 <br /> i <br /> Attention: Guy W.Roy <br /> R&L Diesel Report Page 13 of 41 <br /> -- P.O.Box 2498 <br /> Danville, CA 94526 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sample In ormatio <br /> r Sample ID: BI -44 Sample Type: Grab <br /> F Laboratory ID: 8030609-03 Project Name: UST-Waste Oil <br /> Date/Time Sampled: 06-Mar-08 10:15 by Guy W.Roy Sample Matrix: Soil <br /> :r <br /> Test Parameter Result DLR Unit Dilution B ch Prejmred Analysis Date Method Notes <br /> Tdchloroethene NO 2.00 uglkg 1 AC8 102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Trichlorofluuromethane NO 2.00 ug/kg 1 ACSI710�Mar-06 1 i-Mar-08 EPA 6260B <br /> 1,2,3-Trichloropropane ND 2.00 uglkg 1 ACS 102 11-Altar-08 11-Mar-08 EPA82605 <br /> 1,3,5-Trimethylbemene NO 2.00 ug/kg t AC8 102 11-Mar-08 11-Mar-08 ^ EPA 8260B <br /> v"a 1,2;4-Trimethylbenaene NO 2.00 ug/kg 1 A081102 11-Mar-08 II-Mar-0B EPA 8260B <br /> Vinyl acetate ND 20.0 uglkg 1 AC8 102 11-Mar-08 i I-Mar-08 EPA 8280E <br /> P Ynyl chloride NO 2.00 uglkg 1 AC8 1.02 11-Mar-06 11-Mar-08 EPA 8260E <br /> :� Methyl tart-butyl Ether(WE) NO 2.00 ug/kg 1 AC81102 11-Mar-08 114Mar-oa EPA 8260B <br /> fir= thy[tart-Butyl Ether(ETBE) NO 2.00 ug/kg i ACB�= 11-Mar-08 11-Mar-08 EPA 82608 <br /> p Xylene ND 2.00 uglkg 1 AC8 102 11-Mar OS ^11-Mar 06 EPA 8260E <br /> tart flmyl Methyl Ether(1 AAAE) NO 2.00 uglkg 1 ACB 1102 11-Mar-0B 11-Mar-08 EPA 82608 <br /> o-Xylene ND 2.00 uglkg 1 AC811 102 t 1-Mar-08 11-Mar-08 EPA 8260E - <br /> tert-Butyl Acehol(TBA) NO 50.0 ug/kg 1 AC8I 102 11461ar-08 11-Mar-08 EPA 82608 <br /> f Diisopropyl Ether(DIPE) NO 2.00 ug/kg 1 A081102 11-Mar-08 11-Mar-08 EPA 8260E <br /> '? Surrogate DibromoRuoromethane 54% 86118 <br /> Surrogate:Toluene d8 102% 88-110 <br /> surrogate:4-Broniofluorohenzen8 114% 86-115" µ <br /> n <br /> { <br /> r- <br /> Y <br /> I <br /> 7 <br /> " „rsI-mill7gramr per liter-Ppm DLR=De'ceiiaaLh.KnfarPurmseofRepantng. <br /> ug 2=attcrogmma per Liar—ppb F.xceptianal.tmnpfe matrices ar(ilerfar—c may <br /> result in highCr Atertian llmtts_ <br /> t <br /> RESPECTFULLY SUBMITTED, <br /> ��—J/Ot-z <br /> r <br /> II r <br />' Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave. Stockton, CA 95204 Tel.: 209) 477-8105" Fax: (209) 546-I497 <br />