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tea: <br /> z, i4nalyt►cal Laboratory <br /> CERTIFICATE OFANAL YSIS <br /> Friday,April 4, 2008 <br /> ., <br /> 1, <br /> W.Ro <br /> Guy y <br /> Attention: u <br /> R&L Diesel <br /> 'ZI, Report Page 8 of 41 <br /> P.O.Box 2498 <br /> Danville, CA 94526 <br /> u <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sample Information <br /> Sample ID: B1 -24 Sample Type: Grab <br /> Laboratory ID: 8030609-02 Project Name: UST-Waste Oil <br /> Date/Time Sampled: 06-Mar-08 I0:00 by Guy W,Roy Sample Matrix: Soil <br /> Test Parameter Result DLR Unit Dilution Batch h- ared Anal sis Date Method Notes <br /> Trichloroethene ND 2.00 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Trichlorofluoromethane ND 2.00 ug/kg 1 AC81102 1 i-Mar-08 11-Mar-08 EPA 8260B <br /> 1,2,3-Trichloropropane ND 2.00 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> 1,3,5-Trimethylbenzene ND 2.00 ug/kg 1 AC81102 11-Mar-08 11-Mar-OB EPA 8260E <br /> 1,2,4 Trimethylbenzene ND 2.00 ug/kg 1 AC81102 11-Mar-O8 11-Mar-08 EPA 82608 <br /> '.F <br /> Vinyl acetate ND 20.6 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 82606 <br /> 4` Vinyl chloride ND 2,00 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA$2608 <br /> °r. Methyl tent butyl Ether(MtBE) ND 2.00, uglkg 1 AC81102 11-Mar-08 11-Mar-Q8 EPA 8260B <br /> s„3 rn,p-Xylene 12.8 2.00: ug/kg 1 AC81102 11-Mar-0$ 11-Mar-0B EPA 82$06 <br /> w;= Ethyl tert-Butyl Ether(ETRE) ND 2.00. ug/kg 1 C81 ip217-Mar-08 i 1-Mar-08 EPA 82606 <br /> o-Xylene 18.4 2.00: ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> tert-Amyl Methyl Ether(TAME) ND 2.00, ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 82$0B <br /> tert-Butyl Acohol(TBA) ND 50.0 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> k. .; Diisopropyl Ether(DIPE) ND 2.00: ug/kg 1C81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> ,. <br /> Surrogate:Dibromoftuoromethane 87% 86-118 <br /> Surrogate: Toluene-d8 107%. 88-110 <br /> K's Surrogate.4-8romotluorobenzene 107 W. 86-115 <br /> a' <br /> E?, <br /> mg1L=milligrams per Liter=ppm DLR=Detection Limit forPurpose of Reporting <br /> ug/L—micrograms per Liter=ppb Exceptional sample matrices or interferences may <br /> result in higher detection limits, <br /> RESPECTFULLY SUBMITTED, <br /> r� <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave. Stockton, CA 95204 Tel,: (209) 477-8105 Fax: (209) 546-7497 <br />