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K:. q <br /> LI LJ 1 EUSH O1 , <br /> Analytical Laboratory CERTIFICATE OF ANALYSIS <br /> Friday,April 4, 2008 <br /> Attention: Guy W"Roy <br /> R&L Diesel <br /> P.O.Box 2498 <br /> Report Page 13 of 41 <br /> Danville, CA 94526 <br /> Volatile Organic Compounds by EPA Method 8260B <br /> Sample Inform E tion <br /> Sample ID. B 1 -44 Sample Type: Grab <br /> a Laboratory ID: 8030609-03 Project Name: UST-Waste Oil <br /> 'ri < Date/Time Sampled. 06-Mar-08 10:1 S by Guy W:Roy Sample Matrix: Soil <br /> Test Parameter Result DLR. Unit Dilution Batch Pre aced Analysis Date Method Notes <br /> Trichloroethene ND 2.00 uglkg 1 A,C81102 11-Mar-08 11-Mar-08 EPA 82608 <br /> Trichlorotluoromethane ND 2.00, ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> � <br /> 1,2,3-Trichloropropane ND 2.00� u /k 1 A,,C81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> �< g g <br /> 1,3,5-Trimethylbenzene ND 2.00, uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> 1,2,4-Trimethylbenzene ND 2.00 uglkg 1 A,C81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> z-- <br /> Vinyl acetate ND 20.0` uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E i <br /> " Vinyl chloride ND 2.00. uglkg 1 4C81102 11-Mar-08 11-Mar-08 EPA 8260E I <br /> Methyl tert-butyl Ether(WBE) ND 2.00. uglkg 1 AC81102 11-Mar-08 11-Ma r-08 EPA 8260E <br /> Ethyl tart-Butyl Ether(ETBE) ND 2.00, ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> m,p-Xylene ND 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> tert-Amyl Methyl Ether(TAME) ND 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-OS EPA 8260E <br /> o-Xylene ND 2.00,` uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA$260B <br /> l tert-Butyl Acohol(FBA) ND 50.0 ug/kg 1 AC81102 11-Mar-08 11-Mar-08 EPA 82608 <br /> °' Diisopro I ) ND 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> py Ether(RIPE � - <br /> Surrogate:Dibromofluoromethane 54% 86-118 <br /> ':`:' surrogate:Toluene-d8 102% 88-110 <br /> Surrogate:4-Bromofluotnbenzene 114% 86-115 <br /> mg/L—milligrams per Liter=ppm DLR=Detection o Limit r Purpose+pose ajReporring, <br /> ug,'L=micrograms per Liter=pph F rceptional sample matrices or interferences may <br /> result in higher detection;ltmits. <br /> RESPECTFULLY SUBMITTED, <br /> Jonathan Le,Laboratory Director <br /> 3935 N. Coronado Ave. Stockton, CA 95204 Tel-](209) 477-8105 Fax: (209) 546-7497 <br />