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CERTIFICATE OF ANAL YSIS <br /> ODAnalytical Laboratory Friday,April4, 2008 <br /> > Attention: Guy W.Roy <br /> R&L Diesel Report Page 23 of 41 <br /> P.O.Box 2498 <br /> Danville CA 94526 <br /> Volatile Organic <br /> anic Compounds bY <br /> EPA Method 8260B <br /> ,Y ,Sample Information <br /> »� Sample ID: B2-29 Sample Type: Grab <br /> r <br /> .r Laboratory ID: 8030609-05 Project Name: UST-Waste Oil <br /> r DatvTime Sampled: 06-Mar-08 12:00 by Guy W.Roy Sample Matrix: Sail <br /> Test Parameter Result DLR Unit Mutton Batch Pre aced Ana! sis Date Method Notes <br /> Trichloroethene <br /> ND 2.00 r uglkg 1 Ad81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> , <br /> Tdchlorofluoromethane ND 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> ' 1,2,3-Trichloropropane ND 2,00 uglkg i AC81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> J' <br /> so <br /> 1,3,5-Trimethylbenzene 122 2.00 uglkg 1 A681102 11-Mar-08 11-Mar-08 EPA 82608 <br /> 1 1,2,4-Trimethylbenzene 331 2.00 uglkg 1 AC$1102 11-Mar-08 11-Mar-OS EPA 8260B <br /> Vinyl acetate ND 20.0 uglkg 1 AC81102 11-Mar-08 11-Mar-0B EPA 8260B <br /> fVinyl chloride ND 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> } Methyl tert-butyl Ether(MtBE) ND 2.00 uglkg <br /> 1 A081102 11-Mar-08 11-Mar-08 EPA 8260B <br /> m,p-Xylene 36.6 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA$260B <br /> Ethyl tent-Butyl Ether(ETBE) ND 2.00 uglkg 1 AC81102 11-Mar-0B 11-Mar-08 EPA 82606 <br /> s' tert-Amyl Methyl Ether(TAME) NO 2.00 uglkg 1 AC81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> Yy <br /> o-Xylene 50.8 2.00 uglkg 1 Ab81102 11-Mar-08 11-Mar-08 EPA 8260B <br /> Al;. <br /> [tert-Butyl Acohol(TBA) ND 50.0 uglkg 1 Ab81102 11-Mar-08 11-Mar-08 EPA 8260E <br /> Diisopropyl Ether(DIPE) ND 2.00 uglkg 1 AC81102 11-Mar-O$ 11-Mar O$ EPA 8260E <br /> Surrogate:Dibrornofluoromethane <br /> Surrogate:Tolueno�8 114% . 88 110 <br /> Surrogate:4-Bromofluorobenzene 134% 86-115 <br /> E <br /> mg/L—milligrams per Liter—ppm DLR=Detection Limit far Purpose of Reporting. <br /> ug/L=micrograms per Liter=ppb Exceptional sample matrices ar interferences may <br /> result in higher detectton limits. <br /> RESPECTFULLY SUBMITTED, <br /> S <br /> r� <br /> Jonathan Le,Laboratory Director <br /> .Y 3935 N. Coronado Ave. Stockton, CA 9520.4 Te .: (209) 477-8105 Fax: (209) 546-7497 <br />